(4-chlorophenyl)-carbamic acid (S)-2,2,2-trifluoro-1-[(R)-2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholin-4-ylmethyl]-ethyl ester

Base Information

• Chemical Name: (4-chlorophenyl)-carbamic acid (S)-2,2,2-trifluoro-1-[(R)-2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholin-4-ylmethyl]-ethyl ester
• CAS No.: 1598382-27-4
• Molecular Formula: C₂₁H₂₂ClF₃N₂O₅S
• Molecular Weight: 506.93

Synonyms:(4-chlorophenyl)-carbamic acid (S)-2,2,2-trifluoro-1-[(R)-2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholin-4-ylmethyl]-ethyl ester

Chemical Property of (4-chlorophenyl)-carbamic acid (S)-2,2,2-trifluoro-1-[(R)-2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholin-4-ylmethyl]-ethyl ester

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Technology Process of (4-chlorophenyl)-carbamic acid (S)-2,2,2-trifluoro-1-[(R)-2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholin-4-ylmethyl]-ethyl ester

There total 8 articles about (4-chlorophenyl)-carbamic acid (S)-2,2,2-trifluoro-1-[(R)-2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholin-4-ylmethyl]-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-1,1,1-trifluoro-3-[2-(3-methoxyphenyl)-1,1-dioxo-1λ6-thiomorpholin-4-yl]-propan-2-ol (1598382-97-8) + p-chlorphenylisocyanate (104-12-1) → (4-chlorophenyl)-carbamic acid (S)-2,2,2-trifluoro-1-[(R)-2-(3-methoxyphenyl)-1,1-dioxo-1λ6-thiomorpholin-4-ylmethyl]-ethyl ester (1598382-27-4)

Guidance literature:

In acetonitrile; at 85 ℃;

Reference yield:

tert-butyl 2-(3-methoxyphenyl)thiomorpholine-4-carboxylate (1598382-95-6) → (4-chlorophenyl)-carbamic acid (S)-2,2,2-trifluoro-1-[(R)-2-(3-methoxyphenyl)-1,1-dioxo-1λ6-thiomorpholin-4-ylmethyl]-ethyl ester (1598382-27-4)

Guidance literature:

Multi-step reaction with 4 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.5 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

3: dichloromethane / 20 °C

4: acetonitrile / 85 °C

With 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; In dichloromethane; acetonitrile;

Reference yield:

2-(3-methoxyphenyl)-1,1-dioxo-1λ6-thiomorpholine-4-carboxylic acid tert-butyl ester (1598382-96-7) → (4-chlorophenyl)-carbamic acid (S)-2,2,2-trifluoro-1-[(R)-2-(3-methoxyphenyl)-1,1-dioxo-1λ6-thiomorpholin-4-ylmethyl]-ethyl ester (1598382-27-4)

Guidance literature:

Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2: dichloromethane / 20 °C

3: acetonitrile / 85 °C

With trifluoroacetic acid; In dichloromethane; acetonitrile;

upstream raw materials:

2-(3-methoxyphenyl)thiomorpholine

tert-butyl 2-(3-methoxyphenyl)thiomorpholine-4-carboxylate

2-(3-methoxyphenyl)-1,1-dioxo-1λ⁶-thiomorpholine-4-carboxylic acid tert-butyl ester

2-(3-methoxyphenyl)thiomorpholine1,1-dioxide

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