Technology Process of C36H39N7O6
There total 10 articles about C36H39N7O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
ethanol; toluene;
at 80 ℃;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 20 °C / Cooling with ice
2.1: chloro-trimethyl-silane; triethylamine / N,N-dimethyl-formamide / 100 °C
3.1: hydrogenchloride; water / 19 h / Reflux
4.1: triethylamine; diphenyl phosphoryl azide / N,N-dimethyl-formamide / 7 h / 100 °C
5.1: trifluoroacetic acid / dichloromethane / 5 h / 20 °C
6.1: HATU / N,N-dimethyl-formamide / 1 h / 20 °C
6.2: 20 °C
7.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 8 h / 100 - 110 °C
8.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol / 80 °C / Inert atmosphere
With
hydrogenchloride; chloro-trimethyl-silane; diphenyl phosphoryl azide; water; potassium acetate; sodium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; HATU; trifluoroacetic acid;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0);
In
1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
8.1: Suzuki Coupling;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1.5 h / 20 °C
2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C
2.2: 20 °C
3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol / 80 °C / Inert atmosphere
With
oxalyl dichloride; sodium hydride; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0); N,N-dimethyl-formamide;
In
ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
3.1: Suzuki Coupling;