Technology Process of methyl 2,4,6-triisopropylphenyl sulfoxide
There total 2 articles about methyl 2,4,6-triisopropylphenyl sulfoxide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pentane / 2 h / -78 - 20 °C / Schlenk technique; Inert atmosphere
2: aluminum oxide; Oxone / water; dichloromethane / 4 h / Schlenk technique; Inert atmosphere; Reflux
With
aluminum oxide; Oxone;
In
dichloromethane; water; pentane;
DOI:10.1002/ejic.201700648
- Guidance literature:
-
Triisopropylbenzol, 1) Chlorsulfonierung, 2) Red., 3) Methylierung;
DOI:10.1139/v74-582
- Guidance literature:
-
methyl 2,4,6-triisopropylphenyl sulfoxide;
With
lithium diisopropyl amide;
In
tetrahydrofuran;
at -78 ℃;
for 1h;
Schlenk technique;
Inert atmosphere;
chlorophosphonium;
In
tetrahydrofuran;
at -78 - 20 ℃;
for 1.5h;
Schlenk technique;
Inert atmosphere;
DOI:10.1002/ejic.201700648
