benzaldehyde (10-methyl-6,8-dioxo-4,7-diphenyl-dihydro-1,4-epiazano-[1,2,4]triazolo[1,2-c][1,3,4,5]thiatriazin-2-ylidene)-hydrazone

Base Information

• Chemical Name: benzaldehyde (10-methyl-6,8-dioxo-4,7-diphenyl-dihydro-1,4-epiazano-[1,2,4]triazolo[1,2-c][1,3,4,5]thiatriazin-2-ylidene)-hydrazone
• CAS No.: 61230-67-9
• Molecular Formula: C₂₄H₁₉N₇O₂S
• Molecular Weight: 469.527

Synonyms:benzaldehyde (10-methyl-6,8-dioxo-4,7-diphenyl-dihydro-1,4-epiazano-[1,2,4]triazolo[1,2-c][1,3,4,5]thiatriazin-2-ylidene)-hydrazone

Chemical Property of benzaldehyde (10-methyl-6,8-dioxo-4,7-diphenyl-dihydro-1,4-epiazano-[1,2,4]triazolo[1,2-c][1,3,4,5]thiatriazin-2-ylidene)-hydrazone

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Technology Process of benzaldehyde (10-methyl-6,8-dioxo-4,7-diphenyl-dihydro-1,4-epiazano-[1,2,4]triazolo[1,2-c][1,3,4,5]thiatriazin-2-ylidene)-hydrazone

There total 4 articles about benzaldehyde (10-methyl-6,8-dioxo-4,7-diphenyl-dihydro-1,4-epiazano-[1,2,4]triazolo[1,2-c][1,3,4,5]thiatriazin-2-ylidene)-hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methylbenzothiohydrazide (21048-05-5) → benzaldehyde (10-methyl-6,8-dioxo-4,7-diphenyl-dihydro-1,4-epiazano-[1,2,4]triazolo[1,2-c][1,3,4,5]thiatriazin-2-ylidene)-hydrazone (61230-67-9)

Guidance literature:

Multi-step reaction with 3 steps

1: benzene / Heating

2: NH₃ / CH₂Cl₂

3: acetone / Ambient temperature

With ammonia; In dichloromethane; acetone; benzene;

DOI:10.1039/c39760000439

Reference yield:

5-benzylidenehydrazino-3-methyl-2-phenyl-[1,3,4]thiadiazolium; bromide (71141-06-5) → benzaldehyde (10-methyl-6,8-dioxo-4,7-diphenyl-dihydro-1,4-epiazano-[1,2,4]triazolo[1,2-c][1,3,4,5]thiatriazin-2-ylidene)-hydrazone (61230-67-9)

Guidance literature:

Multi-step reaction with 2 steps

1: NH₃ / CH₂Cl₂

2: acetone / Ambient temperature

With ammonia; In dichloromethane; acetone;

DOI:10.1039/c39760000439

Reference yield:

benzylidene-carbonohydrazonic acid dibromide (1129-63-1) → benzaldehyde (10-methyl-6,8-dioxo-4,7-diphenyl-dihydro-1,4-epiazano-[1,2,4]triazolo[1,2-c][1,3,4,5]thiatriazin-2-ylidene)-hydrazone (61230-67-9)

Guidance literature:

Multi-step reaction with 3 steps

1: benzene / Heating

2: NH₃ / CH₂Cl₂

3: acetone / Ambient temperature

With ammonia; In dichloromethane; acetone; benzene;

DOI:10.1039/c39760000439

upstream raw materials:

4-Phenyl-1,2,4-triazolidine-3,5-dione

5-benzylidenehydrazino-3-methyl-2-phenyl-[1,3,4]thiadiazolium betaine

5-benzylidenehydrazino-3-methyl-2-phenyl-[1,3,4]thiadiazolium; bromide

N-methylbenzothiohydrazide

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