C₄₉H₃₉ClIrNP₂

Base Information

• Chemical Name: C₄₉H₃₉ClIrNP₂
• CAS No.: 1449564-69-5
• Molecular Formula: C₄₉H₃₉ClIrNP₂
• Molecular Weight: 931.476
• Mol file: 1449564-69-5.mol

Synonyms:C₄₉H₃₉ClIrNP₂

Chemical Property of C₄₉H₃₉ClIrNP₂

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₄₉H₃₉ClIrNP₂

There total 3 articles about C₄₉H₃₉ClIrNP₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

bis(1,5-cyclooctadiene)diiridium(I) dichloride (12112-67-3) + 7,8-benzoquinoline (230-27-3) + triphenylphosphine (603-35-0) → C49H39ClIrNP2 (1449564-69-5)

Guidance literature:

In 2-ethoxy-ethanol; for 10h; Schlenk technique; Inert atmosphere; Reflux;

DOI:10.1021/jo401421b

Reference yield: 86.0%

7,8-benzoquinoline (230-27-3) + iridium(III) chloride + water (7732-18-5) + triphenylphosphine (603-35-0) → C49H39ClIrNP2 (1449564-69-5)

Guidance literature:

In 2-ethoxy-ethanol; at 100 ℃; for 8h; Schlenk technique; Inert atmosphere;

Reference yield: 60.0%

7,8-benzoquinoline (230-27-3) + C54H45ClIrP3 (16971-02-1,24846-80-8) → C49H39ClIrNP2 (1449564-69-5)

Guidance literature:

With sodium carbonate; for 3h; Reagent/catalyst; Reflux;

DOI:10.1039/c4tc00466c

upstream raw materials:

bis(1,5-cyclooctadiene)diiridium(I) dichloride

7,8-benzoquinoline

triphenylphosphine

water