Technology Process of C12H10N4O
There total 4 articles about C12H10N4O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 20 ℃;
Cooling with ice;
Inert atmosphere;
DOI:10.1021/ol2008268
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: acetic acid; sodium nitrite / water / 1.5 h / 0 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C / Cooling with ice; Inert atmosphere
With
acetic acid; 3-chloro-benzenecarboperoxoic acid; sodium nitrite;
In
dichloromethane; water;
DOI:10.1021/ol2008268
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / 1,4-dioxane; water / 2.5 h / 80 °C / Inert atmosphere
2.1: acetic acid; sodium nitrite / water / 1.5 h / 0 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C / Cooling with ice; Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; sodium nitrite;
In
1,4-dioxane; dichloromethane; water;
1.1: Suzuki cross-coupling;
DOI:10.1021/ol2008268