6-(1H-indol-4-yl)-4-{5-[(phenylsulfonyl)methyl]-1,3,4-oxadiazol-2-yl}-1H-indazole

Base Information

Chemical Name:6-(1H-indol-4-yl)-4-{5-[(phenylsulfonyl)methyl]-1,3,4-oxadiazol-2-yl}-1H-indazole
CAS No.:1245464-16-7
Molecular Formula:C₂₄H₁₇N₅O₃S
Molecular Weight:455.497
Hs Code.:

Synonyms:6-(1H-indol-4-yl)-4-{5-[(phenylsulfonyl)methyl]-1,3,4-oxadiazol-2-yl}-1H-indazole

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Chemical Property of 6-(1H-indol-4-yl)-4-{5-[(phenylsulfonyl)methyl]-1,3,4-oxadiazol-2-yl}-1H-indazole

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Technology Process of 6-(1H-indol-4-yl)-4-{5-[(phenylsulfonyl)methyl]-1,3,4-oxadiazol-2-yl}-1H-indazole

There total 7 articles about 6-(1H-indol-4-yl)-4-{5-[(phenylsulfonyl)methyl]-1,3,4-oxadiazol-2-yl}-1H-indazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1245465-85-3
C₃₀H₂₁N₅O₅S₂

: 1245464-16-7
6-(1H-indol-4-yl)-4-{5-[(phenylsulfonyl)methyl]-1,3,4-oxadiazol-2-yl}-1H-indazole

Guidance literature:: With water; sodium hydroxide; In isopropyl alcohol; at 20 ℃; for 22h;

Reference yield:

: 1245465-83-1
C₂₅H₁₉N₅O₅S₂

: 1245464-16-7
6-(1H-indol-4-yl)-4-{5-[(phenylsulfonyl)methyl]-1,3,4-oxadiazol-2-yl}-1H-indazole

Guidance literature:: With water; sodium hydroxide; In isopropyl alcohol; at 20 ℃; for 20h;

Reference yield:

: 1245464-68-9
6-bromo-1-(phenylsulfonyl)-1H-indazole-4-carbonitrile

: 1245464-16-7
6-(1H-indol-4-yl)-4-{5-[(phenylsulfonyl)methyl]-1,3,4-oxadiazol-2-yl}-1H-indazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / 1,4-dioxane; water / 3 h / Inert atmosphere; Reflux

2.1: trimethylsilylazide; dibutyl(oxo)stannane / toluene / 90 °C

2.2: 100 °C

3.1: chloroform / 0.5 h / 100 °C / Microwave irradiation

4.1: ethanol / 0.83 h / 100 - 150 °C / Microwave irradiation

5.1: sodium hydroxide / water; isopropyl alcohol / 22 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; trimethylsilylazide; dibutyl(oxo)stannane; sodium hydroxide; In 1,4-dioxane; ethanol; chloroform; water; isopropyl alcohol; toluene;