C₅₇H₉₃N₇O₁₅S₂

Base Information

Chemical Name:C₅₇H₉₃N₇O₁₅S₂
CAS No.:1374760-33-4
Molecular Formula:C₅₇H₉₃N₇O₁₅S₂
Molecular Weight:1180.54
Hs Code.:

C<sub>57</sub>H<sub>93</sub>N<sub>7</sub>O<sub>15</sub>S<sub>2</sub>

Synonyms:C₅₇H₉₃N₇O₁₅S₂

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Chemical Property of C₅₇H₉₃N₇O₁₅S₂

Chemical Property:

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Technology Process of C₅₇H₉₃N₇O₁₅S₂

There total 21 articles about C₅₇H₉₃N₇O₁₅S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374760-17-4
C₂₃H₃₆N₄O₂S₂

: 1374760-32-3
C₃₄H₅₉N₃O₁₄

: 1374760-33-4
C₅₇H₉₃N₇O₁₅S₂

Guidance literature:: C₂₃H₃₆N₄O₂S₂; With dmap; HATU; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h;

C₃₄H₅₉N₃O₁₄; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 0.583333h;

Reference yield:

: 1374760-21-0
C₃₇H₄₄O₈

: 1374760-33-4
C₅₇H₉₃N₇O₁₅S₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

1.2: 2 h / 0 °C

2.1: sodium methylate; methanol / 2 h

2.2: IR-120 (H⁽¹⁺⁾) resin

3.1: triethylamine / acetonitrile / 1.33 h / 0 °C

4.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux

4.2: 20 °C

5.1: tri-n-butyl-tin hydride / Pd(Ph)4 / dichloromethane / 1 h / 20 °C

6.1: hydrogen; acetic acid / palladium 10% on activated carbon / 1,4-dioxane; water / 5 h / 20 °C / 1034.32 Torr

7.1: sodium methylate; methanol / 4 h

7.2: IR-120 (H⁽¹⁺⁾) resin

8.1: 8 h / 80 °C

9.1: dmap; HATU / N,N-dimethyl-formamide / 0.08 h / 0 °C

9.2: 0.58 h / 0 - 20 °C

With methanol; dmap; hydrogen; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; acetic acid; triethylamine; HATU; palladium 10% on activated carbon; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: C₄₃H₅₈O₈Si

: 1374760-33-4
C₅₇H₉₃N₇O₁₅S₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 20 °C

2.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

2.2: 2 h / 0 °C

3.1: sodium methylate; methanol / 2 h

3.2: IR-120 (H⁽¹⁺⁾) resin

4.1: triethylamine / acetonitrile / 1.33 h / 0 °C

5.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux

5.2: 20 °C

6.1: tri-n-butyl-tin hydride / Pd(Ph)4 / dichloromethane / 1 h / 20 °C

7.1: hydrogen; acetic acid / palladium 10% on activated carbon / 1,4-dioxane; water / 5 h / 20 °C / 1034.32 Torr

8.1: sodium methylate; methanol / 4 h

8.2: IR-120 (H⁽¹⁺⁾) resin

9.1: 8 h / 80 °C

10.1: dmap; HATU / N,N-dimethyl-formamide / 0.08 h / 0 °C

10.2: 0.58 h / 0 - 20 °C

With methanol; dmap; tetrabutyl ammonium fluoride; hydrogen; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; acetic acid; triethylamine; HATU; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;