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Technology Process of ((C6H5)CC(C6H5))3WSn(C6H5)3(1-)*N(C2H5)4(1+) = (((C6H5)CC(C6H5))3WSn(C6H5)3)(N(C2H5)4)

((C6H5)CC(C6H5))3WSn(C6H5)3(1-)*N(C2H5)4(1+) = (((C6H5)CC(C6H5))3WSn(C6H5)3)(N(C2H5)4)

Base Information
  • Chemical Name:((C6H5)CC(C6H5))3WSn(C6H5)3(1-)*N(C2H5)4(1+) = (((C6H5)CC(C6H5))3WSn(C6H5)3)(N(C2H5)4)
  • CAS No.:88635-91-0
  • Molecular Formula:C8H20N*C60H45SnW
  • Molecular Weight:1198.83
  • Hs Code.:
((C<sub>6</sub>H<sub>5</sub>)CC(C<sub>6</sub>H<sub>5</sub>))3WSn(C<sub>6</sub>H<sub>5</sub>)3<sup>(1-)</sup>*N(C<sub>2</sub>H<sub>5</sub>)4<sup>(1+)</sup> = (((C<sub>6</sub>H<sub>5</sub>)CC(C<sub>6</sub>H<sub>5</sub>))3WSn(C<sub>6</sub>H<sub>5</sub>)3)(N(C<sub>2</sub>H<sub>5</sub>)4)

Synonyms:((C6H5)CC(C6H5))3WSn(C6H5)3(1-)*N(C2H5)4(1+) = (((C6H5)CC(C6H5))3WSn(C6H5)3)(N(C2H5)4)

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Chemical Property of ((C6H5)CC(C6H5))3WSn(C6H5)3(1-)*N(C2H5)4(1+) = (((C6H5)CC(C6H5))3WSn(C6H5)3)(N(C2H5)4)
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Technology Process of ((C6H5)CC(C6H5))3WSn(C6H5)3(1-)*N(C2H5)4(1+) = (((C6H5)CC(C6H5))3WSn(C6H5)3)(N(C2H5)4)

There total 1 articles about ((C6H5)CC(C6H5))3WSn(C6H5)3(1-)*N(C2H5)4(1+) = (((C6H5)CC(C6H5))3WSn(C6H5)3)(N(C2H5)4) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

((C<sub>6</sub>H<sub>5</sub>)CC(C<sub>6</sub>H<sub>5</sub>))3WSn(C<sub>6</sub>H<sub>5</sub>)3<sup>(1-)</sup>*Li<sup>(1+)</sup> = (((C<sub>6</sub>H<sub>5</sub>)CC(C<sub>6</sub>H<sub>5</sub>))3WSn(C<sub>6</sub>H<sub>5</sub>)3)Li
88635-92-1

((C6H5)CC(C6H5))3WSn(C6H5)3(1-)*Li(1+) = (((C6H5)CC(C6H5))3WSn(C6H5)3)Li

tetraethylammonium bromide
71-91-0

tetraethylammonium bromide

((C<sub>6</sub>H<sub>5</sub>)CC(C<sub>6</sub>H<sub>5</sub>))3WSn(C<sub>6</sub>H<sub>5</sub>)3<sup>(1-)</sup>*N(C<sub>2</sub>H<sub>5</sub>)4<sup>(1+)</sup> = (((C<sub>6</sub>H<sub>5</sub>)CC(C<sub>6</sub>H<sub>5</sub>))3WSn(C<sub>6</sub>H<sub>5</sub>)3)(N(C<sub>2</sub>H<sub>5</sub>)4)
88635-91-0

((C6H5)CC(C6H5))3WSn(C6H5)3(1-)*N(C2H5)4(1+) = (((C6H5)CC(C6H5))3WSn(C6H5)3)(N(C2H5)4)

Guidance literature:
In ethanol; addn. of saturated soln. of anhydrous NEt4Br (2 equiv.) in EtOH to saturated soln. of W-complex in EtOH, ppt. filtered, under dry N2, minimized exposure to light; ppt. washed with water, dried under vac., 3h, recrystd. from acetone at -60°C (recrystd. from CH2Cl2/diethyl ether as CH2Cl2 solvate or from acetone/diethyl ether as diethyl ether solvate; elem. anal.;
DOI:10.1021/ja00320a020
upstream raw materials:

((C6H5)CC(C6H5))3WSn(C6H5)3(1-)*Li(1+) = (((C6H5)CC(C6H5))3WSn(C6H5)3)Li

tetraethylammonium bromide

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