2,2'-Bis(chloromethyl)-4,4'-dimethoxy-3,3',5,5'-tetramethyldiphenylmethane

Base Information

• Chemical Name: 2,2'-Bis(chloromethyl)-4,4'-dimethoxy-3,3',5,5'-tetramethyldiphenylmethane
• CAS No.: 16271-23-1
• Molecular Formula: C₂₁H₂₆Cl₂O₂
• Molecular Weight: 381.342

Synonyms:2,2'-Bis(chloromethyl)-4,4'-dimethoxy-3,3',5,5'-tetramethyldiphenylmethane

Chemical Property of 2,2'-Bis(chloromethyl)-4,4'-dimethoxy-3,3',5,5'-tetramethyldiphenylmethane

Chemical Property:

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Technology Process of 2,2'-Bis(chloromethyl)-4,4'-dimethoxy-3,3',5,5'-tetramethyldiphenylmethane

There total 2 articles about 2,2'-Bis(chloromethyl)-4,4'-dimethoxy-3,3',5,5'-tetramethyldiphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

4,4'-Dimethoxy-3,3',5,5'-tetramethyldiphenylmethane (16271-22-0) + chloromethyl methyl ether (107-30-2) → 2,2'-Bis(chloromethyl)-4,4'-dimethoxy-3,3',5,5'-tetramethyldiphenylmethane (16271-23-1)

Guidance literature:

With titanium tetrachloride; In carbon disulfide; at 0 ℃; for 0.5h;

Reference yield:

→ 2,2'-Bis(chloromethyl)-4,4'-dimethoxy-3,3',5,5'-tetramethyldiphenylmethane (16271-23-1)

Guidance literature:

Bis-(3,5-dimethyl-4-methoxyphenyl)-methan XI, Trioxan/HCl;

Reference yield: 85.0%

2,2'-Bis(chloromethyl)-4,4'-dimethoxy-3,3',5,5'-tetramethyldiphenylmethane (16271-23-1) → 4,4'-Dimethoxy-2,2',3,3',5,5'-hexamethyldiphenylmethane

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 1h; Heating;

upstream raw materials:

4,4'-Dimethoxy-3,3',5,5'-tetramethyldiphenylmethane

chloromethyl methyl ether

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