(+/-)-N-trifluoroacetyl-1-[3,5-dimethoxy-4-(3-phenylpropyl)phenyl]-2-amionopropane

Base Information

Chemical Name:(+/-)-N-trifluoroacetyl-1-[3,5-dimethoxy-4-(3-phenylpropyl)phenyl]-2-amionopropane
CAS No.:289889-88-9
Molecular Formula:C₂₂H₂₆F₃NO₃
Molecular Weight:409.449
Hs Code.:

Synonyms:(+/-)-N-trifluoroacetyl-1-[3,5-dimethoxy-4-(3-phenylpropyl)phenyl]-2-amionopropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-N-trifluoroacetyl-1-[3,5-dimethoxy-4-(3-phenylpropyl)phenyl]-2-amionopropane

Chemical Property:

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Technology Process of (+/-)-N-trifluoroacetyl-1-[3,5-dimethoxy-4-(3-phenylpropyl)phenyl]-2-amionopropane

There total 4 articles about (+/-)-N-trifluoroacetyl-1-[3,5-dimethoxy-4-(3-phenylpropyl)phenyl]-2-amionopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 289889-81-2
(+/-)-N-trifluoroacetyl-1-[3,5-dimethoxy-4-(1-oxo-3-phenylpropy)phenyl]-2-aminopropane

: 289889-88-9
(+/-)-N-trifluoroacetyl-1-[3,5-dimethoxy-4-(3-phenylpropyl)phenyl]-2-amionopropane

Guidance literature:: With perchloric acid; hydrogen; acetic acid; palladium on activated charcoal; for 6h; under 2327.17 Torr;
DOI:10.1021/jm9906062

Reference yield:

: 15402-82-1
1-(3,5-dimethoxyphenyl)propan-2-amine

: 289889-88-9
(+/-)-N-trifluoroacetyl-1-[3,5-dimethoxy-4-(3-phenylpropyl)phenyl]-2-amionopropane

Guidance literature:: Multi-step reaction with 3 steps

1: 33 percent / CH₂Cl₂ / 0.25 h / 20 °C

2: 51 percent / TiCl₄ / CH₂Cl₂ / -30 - 20 °C

3: 65 percent / H₂; AcOH; 70 percent HClO₄ / 10 percent Pd/C / 6 h / 2327.17 Torr

With perchloric acid; hydrogen; titanium tetrachloride; acetic acid; palladium on activated charcoal; In dichloromethane; 1: Acylation / 2: Friedel-Crafts acylation / 3: Reduction;
DOI:10.1021/jm9906062

Reference yield:

: 645-45-4
hydrocinnamic acid chloride

: 289889-88-9
(+/-)-N-trifluoroacetyl-1-[3,5-dimethoxy-4-(3-phenylpropyl)phenyl]-2-amionopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / TiCl₄ / CH₂Cl₂ / -30 - 20 °C

2: 65 percent / H₂; AcOH; 70 percent HClO₄ / 10 percent Pd/C / 6 h / 2327.17 Torr

With perchloric acid; hydrogen; titanium tetrachloride; acetic acid; palladium on activated charcoal; In dichloromethane; 1: Friedel-Crafts acylation / 2: Reduction;
DOI:10.1021/jm9906062