2-((2E,6E,10E)-(R)-14,15-Dihydroxy-3,7,11,15-tetramethyl-hexadeca-2,6,10-trienyl)-6-methyl-[1,4]benzoquinone

Base Information

• Chemical Name: 2-((2E,6E,10E)-(R)-14,15-Dihydroxy-3,7,11,15-tetramethyl-hexadeca-2,6,10-trienyl)-6-methyl-[1,4]benzoquinone
• CAS No.: 865378-57-0
• Molecular Formula: C₂₇H₄₀O₄
• Molecular Weight: 428.612

Synonyms:2-((2E,6E,10E)-(R)-14,15-Dihydroxy-3,7,11,15-tetramethyl-hexadeca-2,6,10-trienyl)-6-methyl-[1,4]benzoquinone

Chemical Property of 2-((2E,6E,10E)-(R)-14,15-Dihydroxy-3,7,11,15-tetramethyl-hexadeca-2,6,10-trienyl)-6-methyl-[1,4]benzoquinone

Chemical Property:

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Technology Process of 2-((2E,6E,10E)-(R)-14,15-Dihydroxy-3,7,11,15-tetramethyl-hexadeca-2,6,10-trienyl)-6-methyl-[1,4]benzoquinone

There total 1 articles about 2-((2E,6E,10E)-(R)-14,15-Dihydroxy-3,7,11,15-tetramethyl-hexadeca-2,6,10-trienyl)-6-methyl-[1,4]benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

2-((2E,6E,10E)-(R)-14,15-Dihydroxy-3,7,11,15-tetramethyl-hexadeca-2,6,10-trienyl)-6-methyl-benzene-1,4-diol → 2-((2E,6E,10E)-(R)-14,15-Dihydroxy-3,7,11,15-tetramethyl-hexadeca-2,6,10-trienyl)-6-methyl-[1,4]benzoquinone (865378-57-0)

Guidance literature:

With ammonium cerium(IV) nitrate; In water; acetonitrile; at 0 ℃; for 0.5h;

DOI:10.1248/bpb.28.374

Reference yield:

2-((2E,6E,10E)-(R)-14,15-Dihydroxy-3,7,11,15-tetramethyl-hexadeca-2,6,10-trienyl)-6-methyl-[1,4]benzoquinone (865378-57-0) → (R)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (4E,8E)-(R)-11-[2,8-dimethyl-6-((R)-3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-2H-chromen-2-yl]-1-(1-hydroxy-1-methyl-ethyl)-4,8-dimethyl-undeca-4,8-dienyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / pyridine / 20 °C

2: 78 percent / pyridine; 4-dimethylaminopyridine / 6 h / 20 °C

With pyridine; dmap;

DOI:10.1248/bpb.28.374

Reference yield:

2-((2E,6E,10E)-(R)-14,15-Dihydroxy-3,7,11,15-tetramethyl-hexadeca-2,6,10-trienyl)-6-methyl-[1,4]benzoquinone (865378-57-0) → (S)-3,3,3-Trifluoro-2-methoxy-2-phenyl-propionic acid (4E,8E)-(R)-11-[2,8-dimethyl-6-((S)-3,3,3-trifluoro-2-methoxy-2-phenyl-propionyloxy)-2H-chromen-2-yl]-1-(1-hydroxy-1-methyl-ethyl)-4,8-dimethyl-undeca-4,8-dienyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / pyridine / 20 °C

2: 79 percent / pyridine; 4-dimethylaminopyridine / 6 h / 20 °C

With pyridine; dmap;

DOI:10.1248/bpb.28.374

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