cis 1-p-tolyl-3-(2'-carbomethoxy-1'-phenoxy methyl)vinylamino-4-p-anisyl-azetidin-2-one

Base Information

Chemical Name:cis 1-p-tolyl-3-(2'-carbomethoxy-1'-phenoxy methyl)vinylamino-4-p-anisyl-azetidin-2-one
CAS No.:77869-34-2
Molecular Formula:C₂₈H₂₈N₂O₅
Molecular Weight:472.541
Hs Code.:

Synonyms:cis 1-p-tolyl-3-(2'-carbomethoxy-1'-phenoxy methyl)vinylamino-4-p-anisyl-azetidin-2-one

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Chemical Property of cis 1-p-tolyl-3-(2'-carbomethoxy-1'-phenoxy methyl)vinylamino-4-p-anisyl-azetidin-2-one

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Technology Process of cis 1-p-tolyl-3-(2'-carbomethoxy-1'-phenoxy methyl)vinylamino-4-p-anisyl-azetidin-2-one

There total 1 articles about cis 1-p-tolyl-3-(2'-carbomethoxy-1'-phenoxy methyl)vinylamino-4-p-anisyl-azetidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3246-78-4
N-(4-methoxybenzylidene)-4-methylaniline

: potassium (2'-carbomethoxy-1'-phenoxy methyl)vinylamino acetate

: 77869-34-2
cis 1-p-tolyl-3-(2'-carbomethoxy-1'-phenoxy methyl)vinylamino-4-p-anisyl-azetidin-2-one

Guidance literature:: With chloroformic acid ethyl ester; triethylamine; Yield given. Multistep reaction; 1.) triethylamine, THF, -25 deg C, 0.5 h 2.) triethylamine, 0.5 h 3.) 1 h;
DOI:10.1002/jhet.5570170808

Reference yield: 52.0%

: 77869-34-2
cis 1-p-tolyl-3-(2'-carbomethoxy-1'-phenoxy methyl)vinylamino-4-p-anisyl-azetidin-2-one

: 50708-29-7
cis 1-p-tolyl-3-phenoxyacetamido-4-p-anisylazetidine 2-one

Guidance literature:: With ruthenium(IV) oxide; sodium periodate; In water; acetone; at 0 ℃; for 0.5h;
DOI:10.1002/jhet.5570170808

Reference yield:

: 77869-34-2
cis 1-p-tolyl-3-(2'-carbomethoxy-1'-phenoxy methyl)vinylamino-4-p-anisyl-azetidin-2-one

: 77869-37-5
N-[(2R,3S)-2-(4-Methoxy-phenyl)-4-oxo-1-p-tolyl-azetidin-3-yl]-2-phenyl-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 52 percent / NaIO₄, RuO₂ / acetone; H₂O / 0.5 h / 0 °C

2: 40 percent / NaIO₄, RuO₂ / acetone; H₂O / 0.5 h / 0 °C

With ruthenium(IV) oxide; sodium periodate; In water; acetone;
DOI:10.1002/jhet.5570170808