Technology Process of 1-(hepta-1,2-dien-1-yl)-4-methoxybenzene
There total 3 articles about 1-(hepta-1,2-dien-1-yl)-4-methoxybenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
iron(III) trifluoride; trifluorormethanesulfonic acid; 2-nitrobenzenesulfonyl hydrazide;
In
nitromethane;
at 20 ℃;
for 0.5h;
DOI:10.1002/chem.201404692
- Guidance literature:
-
butylboronic acid; (E)-N-(3-(4-methoxyphenyl)prop-2-yn-1-ylidene)-2-nitrobenzene sulfonamid;
With
sodium hydride;
at 60 ℃;
for 2h;
Inert atmosphere;
With
tetrabutylammomium bromide; potassium hydroxide;
In
toluene;
at 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1002/chem.201701462
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: scandium tris(trifluoromethanesulfonate) / methanol / 20 °C
2.1: sodium hydride / 2 h / 60 °C / Inert atmosphere
2.2: 12 h / 20 °C / Inert atmosphere
With
sodium hydride; scandium tris(trifluoromethanesulfonate);
In
methanol;
DOI:10.1002/chem.201701462
