C₂₁H₃₄O₅Si

Base Information

Chemical Name:C₂₁H₃₄O₅Si
CAS No.:1388152-91-7
Molecular Formula:C₂₁H₃₄O₅Si
Molecular Weight:394.583
Hs Code.:

C<sub>21</sub>H<sub>34</sub>O<sub>5</sub>Si

Synonyms:C₂₁H₃₄O₅Si

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Chemical Property of C₂₁H₃₄O₅Si

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Technology Process of C₂₁H₃₄O₅Si

There total 10 articles about C₂₁H₃₄O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1388153-24-9
C₂₁H₃₂O₄Si

: 1388152-91-7
C₂₁H₃₄O₅Si

Guidance literature:: With 2,3-Dimethyl-2-butene; dimethyl sulfide borane; In tetrahydrofuran; at 20 ℃; for 0.833333h;
DOI:10.1002/chem.201204303

Reference yield:

: C₂₇H₄₇BO₄Si

: 1388152-91-7
C₂₁H₃₄O₅Si

Guidance literature:: With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 2h;
DOI:10.1021/ja305864z

Reference yield:

: 1388152-89-3
C₁₄H₁₆O₄

: 1388152-91-7
C₂₁H₃₄O₅Si

Guidance literature:: Multi-step reaction with 6 steps

1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.75 h / -78 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 0.67 h / 50 °C

3: diisobutylaluminium hydride / hexane; dichloromethane / 0.75 h / -78 °C / Inert atmosphere

4: 1H-imidazole / N,N-dimethyl-formamide / 20 °C

5: tetrahydrofuran / 0.83 h / 20 °C

6: dihydrogen peroxide; sodium hydroxide / tetrahydrofuran; water / 2 h / 0 - 20 °C

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; dihydrogen peroxide; potassium hexamethylsilazane; diisobutylaluminium hydride; triethylamine; sodium hydroxide; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja305864z