α-[(2E)-2-methyl-3-phenyl-2-propen-1-ylidene]-β-oxo-3,5-bis[[tris(1-methylethyl)silyl]oxy]-(αZ)-benzenepropanoic acid methyl ester

Base Information

• Chemical Name: α-[(2E)-2-methyl-3-phenyl-2-propen-1-ylidene]-β-oxo-3,5-bis[[tris(1-methylethyl)silyl]oxy]-(αZ)-benzenepropanoic acid methyl ester
• CAS No.: 1007842-18-3
• Molecular Formula: C₃₈H₅₈O₅Si₂
• Molecular Weight: 651.047

Synonyms:α-[(2E)-2-methyl-3-phenyl-2-propen-1-ylidene]-β-oxo-3,5-bis[[tris(1-methylethyl)silyl]oxy]-(αZ)-benzenepropanoic acid methyl ester

Chemical Property of α-[(2E)-2-methyl-3-phenyl-2-propen-1-ylidene]-β-oxo-3,5-bis[[tris(1-methylethyl)silyl]oxy]-(αZ)-benzenepropanoic acid methyl ester

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Technology Process of α-[(2E)-2-methyl-3-phenyl-2-propen-1-ylidene]-β-oxo-3,5-bis[[tris(1-methylethyl)silyl]oxy]-(αZ)-benzenepropanoic acid methyl ester

There total 2 articles about α-[(2E)-2-methyl-3-phenyl-2-propen-1-ylidene]-β-oxo-3,5-bis[[tris(1-methylethyl)silyl]oxy]-(αZ)-benzenepropanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

C28H48O4Si2 (1007842-12-7) + C11H13NO (1007842-17-2,1152670-83-1) → α-[(2E)-2-methyl-3-phenyl-2-propen-1-ylidene]-β-oxo-3,5-bis[[tris(1-methylethyl)silyl]oxy]-(αZ)-benzenepropanoic acid methyl ester (1007842-18-3)

Guidance literature:

C₂₈H₄₈O₄Si₂; C₁₁H₁₃NO; In toluene; at 80 ℃; for 16h; Inert atmosphere;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene; at -20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1016/j.tet.2015.05.021

Reference yield:

C39H61NO5Si2 → α-[(2E)-2-methyl-3-phenyl-2-propen-1-ylidene]-β-oxo-3,5-bis[[tris(1-methylethyl)silyl]oxy]-(αZ)-benzenepropanoic acid methyl ester (1007842-18-3)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -20 ℃; for 0.5h;

DOI:10.1021/ja077162g

Reference yield: 80.0%

α-[(2E)-2-methyl-3-phenyl-2-propen-1-ylidene]-β-oxo-3,5-bis[[tris(1-methylethyl)silyl]oxy]-(αZ)-benzenepropanoic acid methyl ester (1007842-18-3) → C38H58O5Si2

Guidance literature:

With copper(II) perchlorate; In 1,2-dichloro-ethane; at 45 ℃; for 8h; Inert atmosphere;

DOI:10.1016/j.tet.2015.05.021

upstream raw materials:

C₂₈H₄₈O₄Si₂

C₁₁H₁₃NO

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