(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*W(CO)4(P(CH₃)3)O₂CCH₃^(1-)

Base Information

Chemical Name:(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*W(CO)4(P(CH₃)3)O₂CCH₃^(1-)
CAS No.:80327-36-2
Molecular Formula:C₉H₁₂O₆PW*C₃₆H₃₀NP₂
Molecular Weight:969.603
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>)3PNP(C<sub>6</sub>H<sub>5</sub>)3<sup>(1+)</sup>*W(CO)4(P(CH<sub>3</sub>)3)O<sub>2</sub>CCH<sub>3</sub><sup>(1-)</sup>

Synonyms:(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*W(CO)4(P(CH₃)3)O₂CCH₃^(1-)

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Chemical Property of (C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*W(CO)4(P(CH₃)3)O₂CCH₃^(1-)

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Technology Process of (C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*W(CO)4(P(CH₃)3)O₂CCH₃^(1-)

There total 3 articles about (C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*W(CO)4(P(CH₃)3)O₂CCH₃^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90388-52-6
cis-[PPN]CH₃W(CO)4P(CH₃)3^(1-)

: 80327-36-2
(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*W(CO)4(P(CH₃)3)O₂CCH₃^(1-)

Guidance literature:: With carbon dioxide; In tetrahydrofuran; excess CO2 (pseudo-first order conditions), 25°C; rate consts. are given; IR data; Kinetics;
DOI:10.1021/ja00311a040

Reference yield:

: PPN⁺W(CO)5(OAc)^-

: 594-09-2
trimethylphosphane

: 80327-36-2
(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*W(CO)4(P(CH₃)3)O₂CCH₃^(1-)

Guidance literature:: In tetrahydrofuran; (N2); to a soln. of the W complex in THF was added P(Me)3, the soln. was heated at about 50°C for 1 h, then cooled to 0°C; filtered, pptd. by the addn. of hexane;

Reference yield:

: [((C₆H₅)3P)2N]⁽¹⁺⁾*[W(CO)4(OCOCH₃)(C₄H₈O)]^(1-)=[((C₆H₅)3P)2N][W(CO)4(OCOCH₃)(C₄H₈O)]

: 594-09-2
trimethylphosphane

: 80327-36-2
(C₆H₅)3PNP(C₆H₅)3⁽¹⁺⁾*W(CO)4(P(CH₃)3)O₂CCH₃^(1-)

Guidance literature:: In not given; to 2.7 mM soln. of (PPN)(W(CO)4(OAc)(THF)) added PMe3 (.approx. 3 equiv.); not isolated, detected by IR spectroscopy;;
DOI:10.1021/ja00278a016