3-{[(tert-butoxy)carbonyl]amino}-4-[(4-methoxybenzyl)selanyl]butanoic acid

Base Information

Chemical Name:3-{[(tert-butoxy)carbonyl]amino}-4-[(4-methoxybenzyl)selanyl]butanoic acid
CAS No.:959415-41-9
Molecular Formula:C₁₇H₂₅NO₅Se
Molecular Weight:402.349
Hs Code.:

Synonyms:3-{[(tert-butoxy)carbonyl]amino}-4-[(4-methoxybenzyl)selanyl]butanoic acid

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Chemical Property of 3-{[(tert-butoxy)carbonyl]amino}-4-[(4-methoxybenzyl)selanyl]butanoic acid

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Technology Process of 3-{[(tert-butoxy)carbonyl]amino}-4-[(4-methoxybenzyl)selanyl]butanoic acid

There total 3 articles about 3-{[(tert-butoxy)carbonyl]amino}-4-[(4-methoxybenzyl)selanyl]butanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 959415-40-8
1-diazo-3-{[(tert-butoxy)carbonyl]amino}-4-[(4-methoxybenzyl)selanyl]butan-2-one

: 959415-41-9
3-{[(tert-butoxy)carbonyl]amino}-4-[(4-methoxybenzyl)selanyl]butanoic acid

Guidance literature:: With water; silver benzoate; In tetrahydrofuran; at 20 ℃; for 4h; ultrasonicated;
DOI:10.1002/hlca.200790171

Reference yield:

: 959415-39-5
(R)-2-((tert-butoxycarbonyl)amino)-3-((4-methoxybenzyl)selanyl)propanoic acid

: 959415-41-9
3-{[(tert-butoxy)carbonyl]amino}-4-[(4-methoxybenzyl)selanyl]butanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Et₃N; ClCO₂iBu / tetrahydrofuran; diethyl ether / 0 - 20 °C

2: 88 percent / PhCO₂Ag; water / tetrahydrofuran / 4 h / 20 °C / ultrasonicated

With water; silver benzoate; triethylamine; isobutyl chloroformate; In tetrahydrofuran; diethyl ether; 2: Wolff rearrangement;
DOI:10.1002/hlca.200790171

Reference yield:

: 146552-76-3
Se-(4-methoxybenzyl)-L-selenocysteine

: 959415-41-9
3-{[(tert-butoxy)carbonyl]amino}-4-[(4-methoxybenzyl)selanyl]butanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 925 mg / aq. NaHCO₃ / acetonitrile

2: 82 percent / Et₃N; ClCO₂iBu / tetrahydrofuran; diethyl ether / 0 - 20 °C

3: 88 percent / PhCO₂Ag; water / tetrahydrofuran / 4 h / 20 °C / ultrasonicated

With water; silver benzoate; sodium hydrogencarbonate; triethylamine; isobutyl chloroformate; In tetrahydrofuran; diethyl ether; acetonitrile; 3: Wolff rearrangement;
DOI:10.1002/hlca.200790171