N-[4-((2S,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylamide

Base Information

Chemical Name:N-[4-((2S,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylamide
CAS No.:135253-88-2
Molecular Formula:C₁₅H₁₉NO₇
Molecular Weight:325.318
Hs Code.:

Synonyms:N-[4-((2S,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylamide

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Chemical Property of N-[4-((2S,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylamide

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Technology Process of N-[4-((2S,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylamide

There total 6 articles about N-[4-((2S,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 91255-92-4
Acetic acid (2S,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(4-acryloylamino-phenoxy)-tetrahydro-pyran-3-yl ester

: 135253-88-2
N-[4-((2S,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylamide

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1039/c39910000536

Reference yield: 95.0%

: 814-68-6,25189-84-8
acryloyl chloride

: 20818-25-1
4-aminophenyl β-D-glucopyranoside

: 135253-88-2
N-[4-((2S,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylamide

Guidance literature:: With triethylamine; In methanol; at 0 ℃;
DOI:10.1039/c39910000536

Reference yield:

: 5987-78-0
p-nitrophenyl 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyde

: 135253-88-2
N-[4-((2S,3R,4S,5S,6R)-3,4,5-Trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-phenyl]-acrylamide

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium formate / 10percent Pd/C / methanol / 0.08 h / Heating

2: NaOMe / methanol

3: 95 percent / Et₃N / methanol / 0 °C

With sodium methylate; ammonium formate; triethylamine; palladium on activated charcoal; In methanol;
DOI:10.1039/c39910000536