1-(4-Chloro-phenyl)-3-[3-(4-chloro-phenyl)-4-hydroxy-4,5,5-trimethyl-2-oxo-imidazolidin-1-yl]-urea

Base Information

• Chemical Name: 1-(4-Chloro-phenyl)-3-[3-(4-chloro-phenyl)-4-hydroxy-4,5,5-trimethyl-2-oxo-imidazolidin-1-yl]-urea
• CAS No.: 85601-65-6
• Molecular Formula: C₁₉H₂₀Cl₂N₄O₃
• Molecular Weight: 423.299

Synonyms:1-(4-Chloro-phenyl)-3-[3-(4-chloro-phenyl)-4-hydroxy-4,5,5-trimethyl-2-oxo-imidazolidin-1-yl]-urea

Chemical Property of 1-(4-Chloro-phenyl)-3-[3-(4-chloro-phenyl)-4-hydroxy-4,5,5-trimethyl-2-oxo-imidazolidin-1-yl]-urea

Chemical Property:

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Technology Process of 1-(4-Chloro-phenyl)-3-[3-(4-chloro-phenyl)-4-hydroxy-4,5,5-trimethyl-2-oxo-imidazolidin-1-yl]-urea

There total 2 articles about 1-(4-Chloro-phenyl)-3-[3-(4-chloro-phenyl)-4-hydroxy-4,5,5-trimethyl-2-oxo-imidazolidin-1-yl]-urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

C19H21Cl2N5O3 (85601-55-4) → 1-(4-Chloro-phenyl)-3-[3-(4-chloro-phenyl)-4-hydroxy-4,5,5-trimethyl-2-oxo-imidazolidin-1-yl]-urea (85601-65-6)

Guidance literature:

With sulfuric acid; In ethanol;

DOI:10.1007/BF00512820

Reference yield:

3-Hydrazino-3-methyl-butan-2-one oxime (61908-01-8) → 1-(4-Chloro-phenyl)-3-[3-(4-chloro-phenyl)-4-hydroxy-4,5,5-trimethyl-2-oxo-imidazolidin-1-yl]-urea (85601-65-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 92 percent / dioxane / 0.17 h

2: 76 percent / H₂SO₄ / ethanol

With sulfuric acid; In 1,4-dioxane; ethanol;

DOI:10.1007/BF00512820

Reference yield: 89.0%

1-(4-Chloro-phenyl)-3-[3-(4-chloro-phenyl)-4-hydroxy-4,5,5-trimethyl-2-oxo-imidazolidin-1-yl]-urea (85601-65-6) → 1-(4-Chloro-phenyl)-3-[3-(4-chloro-phenyl)-5,5-dimethyl-4-methylene-2-oxo-imidazolidin-1-yl]-urea (85601-75-8)

Guidance literature:

In chlorobenzene; Heating;

DOI:10.1007/BF00512820

upstream raw materials:

C₁₉H₂₁Cl₂N₅O₃

3-Hydrazino-3-methyl-butan-2-one oxime

Downstream raw materials:

1-(4-Chloro-phenyl)-3-[3-(4-chloro-phenyl)-5,5-dimethyl-4-methylene-2-oxo-imidazolidin-1-yl]-urea

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