Rh(C₈H₁₂)(((C₆H₅)2PCH₂CH₂)2)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Rh(C₈H₁₂)(((C₆H₅)2PC₂H₄)2)][B(C₆H₅)4]

Base Information

• Chemical Name: Rh(C₈H₁₂)(((C₆H₅)2PCH₂CH₂)2)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Rh(C₈H₁₂)(((C₆H₅)2PC₂H₄)2)][B(C₆H₅)4]
• CAS No.: 154851-55-5
• Molecular Formula: C₂₄H₂₀B*C₃₆H₄₀P₂Rh
• Molecular Weight: 956.8

Synonyms:Rh(C₈H₁₂)(((C₆H₅)2PCH₂CH₂)2)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Rh(C₈H₁₂)(((C₆H₅)2PC₂H₄)2)][B(C₆H₅)4]

Chemical Property of Rh(C₈H₁₂)(((C₆H₅)2PCH₂CH₂)2)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Rh(C₈H₁₂)(((C₆H₅)2PC₂H₄)2)][B(C₆H₅)4]

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Technology Process of Rh(C₈H₁₂)(((C₆H₅)2PCH₂CH₂)2)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Rh(C₈H₁₂)(((C₆H₅)2PC₂H₄)2)][B(C₆H₅)4]

There total 1 articles about Rh(C₈H₁₂)(((C₆H₅)2PCH₂CH₂)2)⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Rh(C₈H₁₂)(((C₆H₅)2PC₂H₄)2)][B(C₆H₅)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

[,14-bis(diphenylphosphino)butane] (1,5-cyclooctadiene)rhodium(I) tetrafluoroborate + sodium tetraphenyl borate (143-66-8) → Rh(C8H12)(((C6H5)2PCH2CH2)2)(1+)*B(C6H5)4(1-)=[Rh(C8H12)(((C6H5)2PC2H4)2)][B(C6H5)4] (154851-55-5)

Guidance literature:

In methanol; N2 or CO-atmosphere; stirring (10 min); washing (H2O, MeOH), drying; elem. anal.;

DOI:10.1021/om960112s

Reference yield: 99.0%

Rh(C8H12)(((C6H5)2PCH2CH2)2)(1+)*B(C6H5)4(1-)=[Rh(C8H12)(((C6H5)2PC2H4)2)][B(C6H5)4] (154851-55-5) → ((C6H5)3BC6H5)Rh(((C6H5)2PCH2CH2)2) (176247-96-4)

Guidance literature:

With hydrogen; In dichloromethane; byproducts: cyclooctane; H2-atmosphere; stirring (room temp., 60 min); hexanes addn., concg., crystn. (N2-atmosphere, room temp., overnight), filtering, washing (CH2Cl2), drying; elem. anal.;

DOI:10.1021/om960112s

upstream raw materials:

sodium tetraphenyl borate

Downstream raw materials:

((C₆H₅)3BC₆H₅)Rh(((C₆H₅)2PCH₂CH₂)2)

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