diethyl p-methylsulfinylbenzylphosphonate

Base Information

Chemical Name:diethyl p-methylsulfinylbenzylphosphonate
CAS No.:118578-87-3
Molecular Formula:C₁₂H₁₉O₄PS
Molecular Weight:290.32
Hs Code.:

Synonyms:diethyl p-methylsulfinylbenzylphosphonate

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Chemical Property of diethyl p-methylsulfinylbenzylphosphonate

Chemical Property:

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Technology Process of diethyl p-methylsulfinylbenzylphosphonate

There total 3 articles about diethyl p-methylsulfinylbenzylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 118578-86-2
diethyl 4-(methylmercapto)benzyl phosphonate

: 118578-87-3
diethyl p-methylsulfinylbenzylphosphonate

Guidance literature:: With dihydrogen peroxide; In acetic acid; for 0.5h; Ambient temperature;
DOI:10.1016/0223-5234(87)90039-0

Reference yield:

: 20074-79-7
diethyl (4-aminobenzyl)phosphonate

: 118578-87-3
diethyl p-methylsulfinylbenzylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 2N HCl, NaNO₂ / H₂O / 1.) -10 deg C, 10 min, 2.) 0 deg C, 20 min

2: H₂O / 1 h / Ambient temperature

3: 90 percent / 30percent H₂O₂ / acetic acid / 0.5 h / Ambient temperature

With hydrogenchloride; dihydrogen peroxide; sodium nitrite; In water; acetic acid;
DOI:10.1016/0223-5234(87)90039-0

Reference yield:

: 4-(Diethoxy-phosphorylmethyl)-benzenediazonium; chloride

: 118578-87-3
diethyl p-methylsulfinylbenzylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂O / 1 h / Ambient temperature

2: 90 percent / 30percent H₂O₂ / acetic acid / 0.5 h / Ambient temperature

With dihydrogen peroxide; In water; acetic acid;
DOI:10.1016/0223-5234(87)90039-0