1-(2,4-difluorobenzyl)-3-(4-fluorophenyl)-6-methyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine trifluoroacetate salt

Base Information

Chemical Name:1-(2,4-difluorobenzyl)-3-(4-fluorophenyl)-6-methyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine trifluoroacetate salt
CAS No.:1427265-61-9
Molecular Formula:C₂HF₃O₂*C₂₀H₁₈F₃N₃
Molecular Weight:471.402
Hs Code.:

Synonyms:1-(2,4-difluorobenzyl)-3-(4-fluorophenyl)-6-methyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine trifluoroacetate salt

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Chemical Property of 1-(2,4-difluorobenzyl)-3-(4-fluorophenyl)-6-methyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine trifluoroacetate salt

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Technology Process of 1-(2,4-difluorobenzyl)-3-(4-fluorophenyl)-6-methyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine trifluoroacetate salt

There total 4 articles about 1-(2,4-difluorobenzyl)-3-(4-fluorophenyl)-6-methyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine trifluoroacetate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 190906-92-4
tert-butyl 2-methyl-4-oxopiperidine-1-carboxylate

: 1427265-61-9
1-(2,4-difluorobenzyl)-3-(4-fluorophenyl)-6-methyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine trifluoroacetate salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

1.2: -78 - 25 °C

2.1: tetrahydrofuran; ethanol / 0.17 h / 25 °C

3.1: hydrogenchloride / 1,4-dioxane / 48 h

4.1: acetonitrile; water

With hydrogenchloride; lithium hexamethyldisilazane; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; water; acetonitrile;

Reference yield:

: C₁₈H₂₂FNO₄

: 1427265-61-9
1-(2,4-difluorobenzyl)-3-(4-fluorophenyl)-6-methyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine trifluoroacetate salt

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; ethanol / 0.17 h / 25 °C

2: hydrogenchloride / 1,4-dioxane / 48 h

3: acetonitrile; water

With hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; ethanol; water; acetonitrile;

Reference yield:

: C₂₅H₂₆F₃N₃O₂

: 1427265-61-9
1-(2,4-difluorobenzyl)-3-(4-fluorophenyl)-6-methyl-4,5,6,7-tetrahydro-1H-pyrazolo[4,3-c]pyridine trifluoroacetate salt

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane / 48 h

2: acetonitrile; water

With hydrogenchloride; In 1,4-dioxane; water; acetonitrile;