tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-α-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->3)-2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside

Base Information

Chemical Name:tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-α-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->3)-2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside
CAS No.:949006-16-0
Molecular Formula:C₆₅H₆₉F₅N₁₂O₁₂Si
Molecular Weight:1333.41
Hs Code.:

tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-α-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->3)-2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside

Synonyms:tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-α-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->3)-2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside

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Chemical Property of tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-α-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->3)-2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside

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Technology Process of tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-α-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->3)-2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside

There total 4 articles about tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-α-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->3)-2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: C₂₃H₂₁O₅N₃F₆

: 949006-15-9
tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->3)-2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside

: 949006-16-0
tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-α-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->3)-2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside

: tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-β-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->3)-2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside

Guidance literature:: With bis(cyclopentadienyl)hafnium dichloride; 4 A molecular sieve; silver perchlorate; In benzene; at 20 ℃; for 5.5h;
DOI:10.1016/j.tet.2007.05.126

Reference yield:

: 904891-28-7
tert-butyldiphenylsilyl 2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside

: 949006-16-0
tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-α-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->3)-2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: AgClO₄; Cp₂HfCl₂; 4 Angstroem molecular sieves / benzene / 6 h / 20 °C

2: 100 percent / NaOMe / methanol; toluene / 0.22 h / 20 °C

3: 93 percent / AgClO₄; Cp₂HfCl₂; 4 Angstroem molecular sieves / benzene / 5.5 h / 20 °C

With bis(cyclopentadienyl)hafnium dichloride; 4 A molecular sieve; sodium methylate; silver perchlorate; In methanol; toluene; benzene;
DOI:10.1016/j.tet.2007.05.126

Reference yield:

: 949005-99-6
C₄₅H₄₈O₈N₉SiF₅

: 949006-16-0
tert-butyldiphenylsilyl 2-azido-3,6-di-O-benzyl-2-deoxy-4-O-pentafluoropropionyl-α-D-galactopyranosyl-(1->4)-2-azido-3,6-di-O-benzyl-2-deoxy-α-D-galactopyranosyl-(1->3)-2,4-diazido-2,4,6-trideoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaOMe / methanol; toluene / 0.22 h / 20 °C

2: 93 percent / AgClO₄; Cp₂HfCl₂; 4 Angstroem molecular sieves / benzene / 5.5 h / 20 °C

With bis(cyclopentadienyl)hafnium dichloride; 4 A molecular sieve; sodium methylate; silver perchlorate; In methanol; toluene; benzene;
DOI:10.1016/j.tet.2007.05.126