C₄₁H₃₆F₂N₂O₇

Base Information

• Chemical Name: C₄₁H₃₆F₂N₂O₇
• CAS No.: 1185883-38-8
• Molecular Formula: C₄₁H₃₆F₂N₂O₇
• Molecular Weight: 706.743
• Mol file: 1185883-38-8.mol

Synonyms:C₄₁H₃₆F₂N₂O₇

Chemical Property of C₄₁H₃₆F₂N₂O₇

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₄₁H₃₆F₂N₂O₇

There total 10 articles about C₄₁H₃₆F₂N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.4%

C41H34F2N2O7 (1185883-42-4) → C41H36F2N2O7 (1185883-38-8)

Guidance literature:

C₄₁H₃₄F₂N₂O₇; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; at 20 ℃; for 0.166667h; Inert atmosphere;

With dimethylsulfide borane complex; In tetrahydrofuran; dichloromethane; for 1.66667h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; methanol; dichloromethane; water; for 0.166667h;

Reference yield: 91.1%

C33H30F2N2O5 (1185883-40-2) + benzyl chloroformate (501-53-1,94274-21-2) → C41H36F2N2O7 (1185883-38-8)

Guidance literature:

With dmap; triethylamine; In dichloromethane; toluene; at 5 - 10 ℃; for 2h;

Reference yield:

C43H40F2N2O8 → C41H36F2N2O7 (1185883-38-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetic acid; sodium dihydrogencitrate / dichloromethane; toluene / 0.58 h / -33 °C

2.1: (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

2.2: 1.67 h / Inert atmosphere

2.3: 0.17 h

With sodium dihydrogencitrate; acetic acid; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; dichloromethane; toluene;

upstream raw materials:

C₄₁H₃₄F₂N₂O₇

benzyl chloroformate

C₃₃H₃₀F₂N₂O₅

N-(4-hydroxybenzylidene)-4-fluorobenzenamine

Downstream raw materials:

C₄₄H₄₄F₂N₂O₇Si