N-(p-bromobenzoylaminomethyl)-N-acetylglycine methyl ester

Base Information

• Chemical Name: N-(p-bromobenzoylaminomethyl)-N-acetylglycine methyl ester
• CAS No.: 172913-10-9
• Molecular Formula: C₁₃H₁₅BrN₂O₄
• Molecular Weight: 343.177
• Mol file: 172913-10-9.mol

Synonyms:N-(p-bromobenzoylaminomethyl)-N-acetylglycine methyl ester

Chemical Property of N-(p-bromobenzoylaminomethyl)-N-acetylglycine methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N-(p-bromobenzoylaminomethyl)-N-acetylglycine methyl ester

There total 1 articles about N-(p-bromobenzoylaminomethyl)-N-acetylglycine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

acetic anhydride (108-24-7) + {[(4-Bromo-benzoylamino)-methyl]-amino}-acetic acid methyl ester; hydrochloride → N-(p-bromobenzoylaminomethyl)-N-acetylglycine methyl ester (172913-10-9)

Guidance literature:

With sodium hydrogencarbonate; for 72h; Ambient temperature;

DOI:10.1007/BF00700898

Reference yield: 84.0%

N-(p-bromobenzoylaminomethyl)-N-acetylglycine methyl ester (172913-10-9) → N-[(Acetyl-carbamoylmethyl-amino)-methyl]-4-bromo-benzamide

Guidance literature:

With ammonia; In isopropyl alcohol; at 20 ℃;

DOI:10.1007/BF01431807

Reference yield: 73.0%

N-(p-bromobenzoylaminomethyl)-N-acetylglycine methyl ester (172913-10-9) → {Acetyl-[(4-bromo-benzoylamino)-methyl]-amino}-acetic acid (184246-11-5)

Guidance literature:

With sodium hydroxide; In water; 1) 60-70 deg C, 2) 20 deg C, 24 h;

DOI:10.1007/BF01431807

upstream raw materials:

acetic anhydride

Downstream raw materials:

{Acetyl-[(4-bromo-benzoylamino)-methyl]-amino}-acetic acid