(E)-N'-(1-(2-bromophenyl)-2-(phenylamino)ethylidene)-4-methylbenzenesulfonohydrazide

Base Information

• Chemical Name: (E)-N'-(1-(2-bromophenyl)-2-(phenylamino)ethylidene)-4-methylbenzenesulfonohydrazide
• CAS No.: 1258383-63-9
• Molecular Formula: C₂₁H₂₀BrN₃O₂S
• Molecular Weight: 458.379
• Mol file: 1258383-63-9.mol

Synonyms:(E)-N'-(1-(2-bromophenyl)-2-(phenylamino)ethylidene)-4-methylbenzenesulfonohydrazide

Chemical Property of (E)-N'-(1-(2-bromophenyl)-2-(phenylamino)ethylidene)-4-methylbenzenesulfonohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-N'-(1-(2-bromophenyl)-2-(phenylamino)ethylidene)-4-methylbenzenesulfonohydrazide

There total 1 articles about (E)-N'-(1-(2-bromophenyl)-2-(phenylamino)ethylidene)-4-methylbenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

C15H14Br2N2O2S (1276043-59-4) + aniline (62-53-3) → (E)-N'-(1-(2-bromophenyl)-2-(phenylamino)ethylidene)-4-methylbenzenesulfonohydrazide (1258383-63-9) + (N',N''E,N',N''E)-N',N''-(2,2'-(phenylazanediyl)bis(1-(2-bromophenyl)ethan-2-yl-1-ylidene))bis(4-methylbenzenesulfonohydrazide) (1258383-61-7)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In water; acetonitrile; at 20 ℃; for 0.5h;

DOI:10.1016/j.tet.2010.09.069

Reference yield: 100.0%

(E)-N'-(1-(2-bromophenyl)-2-(phenylamino)ethylidene)-4-methylbenzenesulfonohydrazide (1258383-63-9) → N-((1-tosyl-1H-indazol-3-yl)methyl)aniline (1258383-80-0)

Guidance literature:

(E)-N'-(1-(2-bromophenyl)-2-(phenylamino)ethylidene)-4-methylbenzenesulfonohydrazide; With sodium carbonate; In ethanol; water; at 20 ℃; for 0.0333333h;

With copper(l) iodide; N,N`-dimethylethylenediamine; In ethanol; water; at 20 ℃; for 0.166667h;

DOI:10.1016/j.tet.2010.09.069

upstream raw materials:

C₁₅H₁₄Br₂N₂O₂S

aniline

Downstream raw materials:

N-((1-tosyl-1H-indazol-3-yl)methyl)aniline