C₁₂H₁₀F₃NOSe

Base Information

• Chemical Name: C₁₂H₁₀F₃NOSe
• CAS No.: 1332498-00-6
• Molecular Formula: C₁₂H₁₀F₃NOSe
• Molecular Weight: 320.173
• Mol file: 1332498-00-6.mol

Synonyms:C₁₂H₁₀F₃NOSe

Chemical Property of C₁₂H₁₀F₃NOSe

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₂H₁₀F₃NOSe

There total 3 articles about C₁₂H₁₀F₃NOSe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

C14H12F3NO2Se (1332497-99-0) → C12H10F3NOSe (1332498-00-6)

Guidance literature:

With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 - -10 ℃; for 1.5h; Inert atmosphere;

Reference yield:

4-CF3C6H4CN (455-18-5) → C12H10F3NOSe (1332498-00-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: hydrogenchloride; pyridine / ethanol / 2 h / Inert atmosphere; Reflux

2.1: tetrahydrofuran / 12.83 h / 20 - 80 °C / Reflux

2.2: 0.33 h / 20 °C

3.1: diisobutylaluminium hydride / dichloromethane; hexane / 1.5 h / -78 - -10 °C / Inert atmosphere

With pyridine; hydrogenchloride; diisobutylaluminium hydride; In tetrahydrofuran; ethanol; hexane; dichloromethane;

Reference yield:

4-(trifluoromethyl)benzoselenoamide (1332497-98-9) → C12H10F3NOSe (1332498-00-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 12.83 h / 20 - 80 °C / Reflux

1.2: 0.33 h / 20 °C

2.1: diisobutylaluminium hydride / dichloromethane; hexane / 1.5 h / -78 - -10 °C / Inert atmosphere

With diisobutylaluminium hydride; In tetrahydrofuran; hexane; dichloromethane;

upstream raw materials:

4-CF₃C₆H₄CN

4-(trifluoromethyl)benzoselenoamide

C₁₄H₁₂F₃NO₂Se

Downstream raw materials:

C₁₉H₁₆F₃NO₃SSe

C₁₂H₉ClF₃NSe

C₁₂H₁₁F₃N₂Se

C₁₉H₁₆F₃NOSSe