2-hydroxybakuchiol methyl ether

Base Information

Chemical Name:2-hydroxybakuchiol methyl ether
CAS No.:74921-97-4
Molecular Formula:C₁₉H₂₈O₂
Molecular Weight:288.43
Hs Code.:

Synonyms:2-hydroxybakuchiol methyl ether

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Chemical Property of 2-hydroxybakuchiol methyl ether

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Technology Process of 2-hydroxybakuchiol methyl ether

There total 3 articles about 2-hydroxybakuchiol methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 2,3-epoxybakuchiol methyl ether

: 74921-97-4
2-hydroxybakuchiol methyl ether

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; 1.) 0 deg C, 0.5 h, 2.) reflux, 4 h;
DOI:10.1271/bbb1961.44.1483

Reference yield:

: 17015-63-3,100428-91-9,10309-44-1
(S,E)-1-(3,7-dimethyl-3-vinylocta-1,6-dien-1-yl)-4-methoxybenzene

: 74921-97-4
2-hydroxybakuchiol methyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: perbenzoic acid / benzene / 14 h / 0 - 5 °C

2: 87 percent / LiAlH₄ / tetrahydrofuran / 1.) 0 deg C, 0.5 h, 2.) reflux, 4 h

With lithium aluminium tetrahydride; Perbenzoic acid; In tetrahydrofuran; benzene;
DOI:10.1271/bbb1961.44.1483

Reference yield:

: 17015-60-0,93998-10-8,10309-37-2
bakuchiol

: 74921-97-4
2-hydroxybakuchiol methyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / tetrahydrofuran / 1.) r.t., 0.5 h, 2.) reflux, 6 h

2: perbenzoic acid / benzene / 14 h / 0 - 5 °C

3: 87 percent / LiAlH₄ / tetrahydrofuran / 1.) 0 deg C, 0.5 h, 2.) reflux, 4 h

With lithium aluminium tetrahydride; Perbenzoic acid; sodium hydride; In tetrahydrofuran; benzene;
DOI:10.1271/bbb1961.44.1483