C₁₀H₉F₃O₂

Base Information

Chemical Name:C₁₀H₉F₃O₂
CAS No.:143072-25-7
Molecular Formula:C₁₀H₉F₃O₂
Molecular Weight:218.175
Hs Code.:

C<sub>10</sub>H<sub>9</sub>F<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₀H₉F₃O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₀H₉F₃O₂

Chemical Property:

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Technology Process of C₁₀H₉F₃O₂

There total 2 articles about C₁₀H₉F₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1180131-27-4
α-CF3 hydrocinnamaldehyde

: 143072-25-7
C₁₀H₉F₃O₂

Guidance literature:: With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In dichloromethane; water; N,N-dimethyl-formamide; at -20 ℃; for 2h; optical yield given as %ee;
DOI:10.1021/ja9053338

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 143072-25-7
C₁₀H₉F₃O₂

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-dimethylpyridine; Ir(ppy)2(dtb-bpy)PF₆; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt / N,N-dimethyl-formamide / 7.5 h / -20 °C / fluorescent light

2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water; N,N-dimethyl-formamide / 2 h / -20 °C

With 2,6-dimethylpyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; Ir(ppy)2(dtb-bpy)PF₆; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja9053338

Reference yield:

: 143072-25-7
C₁₀H₉F₃O₂

: 865-47-4
potassium tert-butylate

: 1180131-24-1
C₁₄H₁₈F₃NO₂

Guidance literature:: With diphenyl phosphoryl azide; In tert-butyl alcohol; at 110 ℃; for 10h; optical yield given as %ee; Inert atmosphere; Molecular sieve;
DOI:10.1021/ja9053338