5-(3-CHLOROPHENYL)-4-(2,4-DICHLOROPHENYL)-4H-1,2,4-TRIAZOLE-3-THIOL

Base Information

• Chemical Name: 5-(3-CHLOROPHENYL)-4-(2,4-DICHLOROPHENYL)-4H-1,2,4-TRIAZOLE-3-THIOL
• CAS No.: 885267-50-5
• Molecular Formula: C₁₄H₈Cl₃N₃S
• Molecular Weight: 356.663
• Hs Code.: 2933998090
• Mol file: 885267-50-5.mol

Synonyms:4-(2,4-dichlorophenyl)-5-(3-chlorophenyl)-2,4-dihydro-3H-1,2,4-triazole-3-thione

Chemical Property of 5-(3-CHLOROPHENYL)-4-(2,4-DICHLOROPHENYL)-4H-1,2,4-TRIAZOLE-3-THIOL

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

5-(3-Chlorophenyl)-4-(2,4-dichlorophenyl)-4H-1,2,4-triazole-3-thiol ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

Useful:

Technology Process of 5-(3-CHLOROPHENYL)-4-(2,4-DICHLOROPHENYL)-4H-1,2,4-TRIAZOLE-3-THIOL

There total 4 articles about 5-(3-CHLOROPHENYL)-4-(2,4-DICHLOROPHENYL)-4H-1,2,4-TRIAZOLE-3-THIOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

C14H10Cl3N3OS (891642-93-6) → 4-(2,4-dichlorophenyl)-5-(3-chlorophenyl)-2,4-dihydro-3H-1,2,4-triazole-3-thione (885267-50-5)

Guidance literature:

With sodium hydroxide; for 2h; Reflux;

DOI:10.2174/15701808113109990082

Reference yield:

3-chlorobenzhydrazide (1673-47-8) → 4-(2,4-dichlorophenyl)-5-(3-chlorophenyl)-2,4-dihydro-3H-1,2,4-triazole-3-thione (885267-50-5)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 0.08 h / Reflux

2: sodium hydroxide / Reflux

With sodium hydroxide; In ethanol;

DOI:10.1016/j.ejmech.2012.11.040

Reference yield:

2, 4-dichlorophenyl isothiocyanate (6590-96-1) → 4-(2,4-dichlorophenyl)-5-(3-chlorophenyl)-2,4-dihydro-3H-1,2,4-triazole-3-thione (885267-50-5)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol / 0.08 h / Reflux

2: sodium hydroxide / Reflux

With sodium hydroxide; In ethanol;

DOI:10.1016/j.ejmech.2012.11.040

upstream raw materials:

3-chlorobenzhydrazide

2, 4-dichlorophenyl isothiocyanate

C₁₄H₁₀Cl₃N₃OS

Downstream raw materials:

C₃₂H₂₆Cl₃FN₆O₃S