(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))](PF₆)

Base Information

• Chemical Name: (C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))](PF₆)
• CAS No.: 174737-94-1
• Molecular Formula: C₂₄H₂₈CoO₃*F₆P
• Molecular Weight: 568.442

Synonyms:(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))](PF₆)

Chemical Property of (C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))](PF₆)

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Technology Process of (C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))](PF₆)

There total 1 articles about (C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOH))](PF₆) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

ammonium hexafluorophosphate + (C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(COOC2H5))(1+)*PF6(1-) = [(C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(COOC2H5))](PF6) (174737-90-7) → (C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(COOH))(1+)*PF6(1-) = [(C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(COOH))](PF6) (174737-94-1)

Guidance literature:

With NaH; aq. HCl; In hydrogenchloride; (N2 or Ar); stirring (80°C, 24 h), addn. of NH4PF6; recrystn. (EtOH); elem. anal.;

DOI:10.1246/bcsj.69.17

Reference yield: 82.0%

ammonium hexafluorophosphate + (C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(COOH))(1+)*PF6(1-) = [(C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(COOH))](PF6) (174737-94-1) + aniline (62-53-3) → (C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(CONHC6H5))(1+)*PF6(1-) = [(C5(CH3)5)Co(C5H2(OC2H5)(C6H5)(CONHC6H5))](PF6) (174737-98-5)

Guidance literature:

With thionyl chloride; In acetonitrile; (N2 or Ar); stirring complex with thionyl chloride, aniline in MeCN addn., stirring (room temp., overnight), evapn., NH4PF6 in meOH addn.; recrystn. (MeOH); elem. anal.;

DOI:10.1246/bcsj.69.17

upstream raw materials:

(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(COOC₂H₅))](PF₆)

Downstream raw materials:

(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(CONHC₆H₅))⁽¹⁺⁾*PF₆^(1-) = [(C₅(CH₃)5)Co(C₅H₂(OC₂H₅)(C₆H₅)(CONHC₆H₅))](PF₆)

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