DL-α-hydroxy-4-(p-methoxybenzyloxycarbonyl)phenylacetic acid

Base Information

• Chemical Name: DL-α-hydroxy-4-(p-methoxybenzyloxycarbonyl)phenylacetic acid
• CAS No.: 59207-74-8
• Molecular Formula: C₁₇H₁₆O₆
• Molecular Weight: 316.31
• Mol file: 59207-74-8.mol

Synonyms:DL-α-hydroxy-4-(p-methoxybenzyloxycarbonyl)phenylacetic acid

Chemical Property of DL-α-hydroxy-4-(p-methoxybenzyloxycarbonyl)phenylacetic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of DL-α-hydroxy-4-(p-methoxybenzyloxycarbonyl)phenylacetic acid

There total 2 articles about DL-α-hydroxy-4-(p-methoxybenzyloxycarbonyl)phenylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dipotassium salt of DL-α-hydroxy-4-carboxyphenylacetic acid + phenolphthalein (77-09-8) + p-methoxybenzyl chloride (824-94-2) → DL-α-hydroxy-4-(p-methoxybenzyloxycarbonyl)phenylacetic acid (59207-74-8)

Guidance literature:

In ice-water; dimethyl sulfoxide; ethyl acetate; acetone; benzene;

Reference yield:

→ DL-α-hydroxy-4-(p-methoxybenzyloxycarbonyl)phenylacetic acid (59207-74-8)

Guidance literature:

aus Di-K-Salz der DL-α-Hydroxy-4-carboxy-phenyl-essigsaeure in DMSO, 1) p-Methoxy-benzylchlorid, 2) Eiswasser (pH 7,5), 3) Aethylacetat, 4) NaOH, 5) HCl;

Reference yield:

DL-α-hydroxy-4-(p-methoxybenzyloxycarbonyl)phenylacetic acid (59207-74-8) → DL-α-chloroacetoxy-4-(p-methoxybenzyloxycarbonyl)phenylacetic acid (59207-75-9)

Guidance literature:

In ice-water; dichloromethane; benzene;

upstream raw materials:

phenolphthalein

p-methoxybenzyl chloride

Downstream raw materials:

DL-α-chloroacetoxy-4-(p-methoxybenzyloxycarbonyl)phenylacetic acid

Refernces