methyl 2-deoxy-2-C-methyl-3-O-methyl-6-O-triphenylmethyl-α-D-xylo-hexapyranosid-4-ulose

Base Information

Chemical Name:methyl 2-deoxy-2-C-methyl-3-O-methyl-6-O-triphenylmethyl-α-D-xylo-hexapyranosid-4-ulose
CAS No.:64526-85-8
Molecular Formula:C₂₈H₃₀O₅
Molecular Weight:446.543
Hs Code.:

Synonyms:methyl 2-deoxy-2-C-methyl-3-O-methyl-6-O-triphenylmethyl-α-D-xylo-hexapyranosid-4-ulose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-deoxy-2-C-methyl-3-O-methyl-6-O-triphenylmethyl-α-D-xylo-hexapyranosid-4-ulose

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Technology Process of methyl 2-deoxy-2-C-methyl-3-O-methyl-6-O-triphenylmethyl-α-D-xylo-hexapyranosid-4-ulose

There total 15 articles about methyl 2-deoxy-2-C-methyl-3-O-methyl-6-O-triphenylmethyl-α-D-xylo-hexapyranosid-4-ulose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 64526-84-7,64526-85-8
methyl 2-deoxy-2-C-methyl-3-O-methyl-6-O-triphenylmethyl-α-D-ribo-hexapyranosid-4-ulose

: 64526-85-8
methyl 2-deoxy-2-C-methyl-3-O-methyl-6-O-triphenylmethyl-α-D-xylo-hexapyranosid-4-ulose

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1021/ja00386a076

Reference yield:

: 64526-83-6
methyl 2-deoxy-2-C-methyl-3-O-methyl-6-O-triphenylmethyl-α-D-allopyranoside

: 64526-84-7,64526-85-8
methyl 2-deoxy-2-C-methyl-3-O-methyl-6-O-triphenylmethyl-α-D-ribo-hexapyranosid-4-ulose

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In pyridine; dimethyl sulfoxide; trifluoroacetic acid; for 18h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4020(01)82415-7

Reference yield:

: 64526-83-6
methyl 2-deoxy-2-C-methyl-3-O-methyl-6-O-triphenylmethyl-α-D-allopyranoside

: 64526-85-8
methyl 2-deoxy-2-C-methyl-3-O-methyl-6-O-triphenylmethyl-α-D-xylo-hexapyranosid-4-ulose

Guidance literature:: Multi-step reaction with 2 steps

1: ethyldimethylaminopropyl carbodiimide, HCl / dimethylsulfoxide

2: 85 percent / NaOMe / methanol

With hydrogenchloride; sodium methylate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In methanol; dimethyl sulfoxide;
DOI:10.1021/ja00386a076