2,3',6-trihydroxy-4-<1-(carbo-tert-butoxy)-3,4-dihydroxybutoxy>-4'-methoxydihydrochalcone

Base Information

Chemical Name:2,3',6-trihydroxy-4-<1-(carbo-tert-butoxy)-3,4-dihydroxybutoxy>-4'-methoxydihydrochalcone
CAS No.:76799-45-6
Molecular Formula:C₂₅H₃₂O₁₀
Molecular Weight:492.523
Hs Code.:

Synonyms:2,3',6-trihydroxy-4-<1-(carbo-tert-butoxy)-3,4-dihydroxybutoxy>-4'-methoxydihydrochalcone

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Chemical Property of 2,3',6-trihydroxy-4-<1-(carbo-tert-butoxy)-3,4-dihydroxybutoxy>-4'-methoxydihydrochalcone

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Technology Process of 2,3',6-trihydroxy-4-<1-(carbo-tert-butoxy)-3,4-dihydroxybutoxy>-4'-methoxydihydrochalcone

There total 4 articles about 2,3',6-trihydroxy-4-<1-(carbo-tert-butoxy)-3,4-dihydroxybutoxy>-4'-methoxydihydrochalcone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 76799-44-5
2,3',6-tris(benzyloxy)-4-<1-(carbo-tert-butoxy)-3,4-dihydroxybutoxy>-4'-methoxydihydrochalcone

: 76799-45-6
2,3',6-trihydroxy-4-<1-(carbo-tert-butoxy)-3,4-dihydroxybutoxy>-4'-methoxydihydrochalcone

Guidance literature:: With hydrogen; palladium on activated charcoal; In dichloromethane; tert-butyl alcohol; for 19h; under 2660 Torr; Ambient temperature;
DOI:10.1021/jm00136a011

Reference yield:

: 39149-84-3
tert-butyl 2-bromo-4-pentenoate

: 76799-45-6
2,3',6-trihydroxy-4-<1-(carbo-tert-butoxy)-3,4-dihydroxybutoxy>-4'-methoxydihydrochalcone

Guidance literature:: Multi-step reaction with 4 steps

1: 59 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 14 h / Ambient temperature

2: 100 percent / K₂CO₃ / dimethylformamide / 86 h / Ambient temperature

3: 67 percent / aq. H₂SO₄ / dioxane / 40 h / Ambient temperature

4: 74 percent / H₂ / Pd/C / 2-methyl-propan-2-ol; CH₂Cl₂ / 19 h / 2660 Torr / Ambient temperature

With sulfuric acid; hydrogen; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jm00136a011

Reference yield:

: 76799-42-3
tert-butyl 2-bromo-4,5-epoxypentanoate

: 76799-45-6
2,3',6-trihydroxy-4-<1-(carbo-tert-butoxy)-3,4-dihydroxybutoxy>-4'-methoxydihydrochalcone

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / K₂CO₃ / dimethylformamide / 86 h / Ambient temperature

2: 67 percent / aq. H₂SO₄ / dioxane / 40 h / Ambient temperature

3: 74 percent / H₂ / Pd/C / 2-methyl-propan-2-ol; CH₂Cl₂ / 19 h / 2660 Torr / Ambient temperature

With sulfuric acid; hydrogen; potassium carbonate; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/jm00136a011