C₂₉H₃₀N₂O₅

Base Information

• Chemical Name: C₂₉H₃₀N₂O₅
• CAS No.: 1565836-81-8
• Molecular Formula: C₂₉H₃₀N₂O₅
• Molecular Weight: 486.568
• Mol file: 1565836-81-8.mol

Synonyms:C₂₉H₃₀N₂O₅

Chemical Property of C₂₉H₃₀N₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₃₀N₂O₅

There total 12 articles about C₂₉H₃₀N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C35H44N2O5Si (1565836-80-7) → C29H30N2O5 (1565836-81-8)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -78 - 25 ℃; for 1h;

DOI:10.1021/ja500548e

Reference yield:

C34H44N2O5Si → C29H30N2O5 (1565836-81-8)

Guidance literature:

Multi-step reaction with 10 steps

1.1: acetic acid; sodium cyanoborohydride / isopropyl alcohol / 16 h / 25 °C

2.1: hydrogen

3.1: ChiralCel OD column / isopropyl alcohol; hexane / Resolution of racemate

4.1: 1H-imidazole; sodium hydride / tetrahydrofuran; mineral oil / 0 - 25 °C

4.2: 1 h / 0 - 25 °C

4.3: 1 h / 0 - 25 °C

5.1: toluene / 36 h / 150 °C

6.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

6.2: 2.5 h / -78 °C

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 - 25 °C

8.1: Lawessons reagent / toluene / 0.5 h / 100 °C / Inert atmosphere

9.1: 2,6-di-tert-butyl-pyridine; trimethoxonium tetrafluoroborate / dichloromethane / 12 h / 25 °C / Inert atmosphere

9.2: 0.75 h / 0 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / -78 - 25 °C

With Lawessons reagent; 1H-imidazole; 2,6-di-tert-butyl-pyridine; tetrabutyl ammonium fluoride; hydrogen; trimethoxonium tetrafluoroborate; sodium hydride; sodium cyanoborohydride; acetic acid; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; isopropyl alcohol; toluene; mineral oil;

DOI:10.1021/ja500548e

Reference yield:

C35H42N2O6Si → C29H30N2O5 (1565836-81-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: ChiralCel OD column / isopropyl alcohol; hexane / Resolution of racemate

2.1: 2,6-di-tert-butyl-pyridine; trimethoxonium tetrafluoroborate / dichloromethane / 12 h / 25 °C / Inert atmosphere

2.2: 0.75 h / 0 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / -78 - 25 °C

With 2,6-di-tert-butyl-pyridine; tetrabutyl ammonium fluoride; trimethoxonium tetrafluoroborate; In tetrahydrofuran; hexane; dichloromethane; isopropyl alcohol;

DOI:10.1021/ja500548e

upstream raw materials:

C₃₅H₄₆N₂O₇Si

C₃₇H₄₈N₂O₇S₂Si

C₃₅H₄₄N₂O₅Si

C₃₅H₄₂N₂O₅SSi

Downstream raw materials:

C₂₉H₂₉IN₂O₄