5-benzyl 1,2,3,4-tetrahydro-2,2-dimethyl-4-oxo-10H-phenothiazin-5-ium picrate

Base Information

Chemical Name:5-benzyl 1,2,3,4-tetrahydro-2,2-dimethyl-4-oxo-10H-phenothiazin-5-ium picrate
CAS No.:137411-48-4
Molecular Formula:C₆H₂N₃O₇*C₂₁H₂₂NOS
Molecular Weight:564.576
Hs Code.:

Synonyms:5-benzyl 1,2,3,4-tetrahydro-2,2-dimethyl-4-oxo-10H-phenothiazin-5-ium picrate

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Chemical Property of 5-benzyl 1,2,3,4-tetrahydro-2,2-dimethyl-4-oxo-10H-phenothiazin-5-ium picrate

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Technology Process of 5-benzyl 1,2,3,4-tetrahydro-2,2-dimethyl-4-oxo-10H-phenothiazin-5-ium picrate

There total 4 articles about 5-benzyl 1,2,3,4-tetrahydro-2,2-dimethyl-4-oxo-10H-phenothiazin-5-ium picrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126-81-8
dimedone

: 137411-48-4
5-benzyl 1,2,3,4-tetrahydro-2,2-dimethyl-4-oxo-10H-phenothiazin-5-ium picrate

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / toluene-4-sulphonic acid / toluene / 18 h / Heating

2: 59 percent / 30percent aq. H₂O₂, acetic acid / CH₂Cl₂ / 18 h / Ambient temperature

3: 1) trifluoroactic anhydride / 1) dichloromethane, -61 deg C, 2.5 h, 2) room temp., overnight

With dihydrogen peroxide; toluene-4-sulfonic acid; acetic acid; trifluoroacetic anhydride; In dichloromethane; toluene;

Reference yield:

: 137411-43-9
3-(2-benzylthioanilino)-5,5-dimethylcyclohex-2-enone

: 137411-48-4
5-benzyl 1,2,3,4-tetrahydro-2,2-dimethyl-4-oxo-10H-phenothiazin-5-ium picrate

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / 30percent aq. H₂O₂, acetic acid / CH₂Cl₂ / 18 h / Ambient temperature

2: 1) trifluoroactic anhydride / 1) dichloromethane, -61 deg C, 2.5 h, 2) room temp., overnight

With dihydrogen peroxide; acetic acid; trifluoroacetic anhydride; In dichloromethane;

Reference yield:

: 6325-92-4
2-(benzylsulfanyl)aniline

: 137411-48-4
5-benzyl 1,2,3,4-tetrahydro-2,2-dimethyl-4-oxo-10H-phenothiazin-5-ium picrate

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / toluene-4-sulphonic acid / toluene / 18 h / Heating

2: 59 percent / 30percent aq. H₂O₂, acetic acid / CH₂Cl₂ / 18 h / Ambient temperature

3: 1) trifluoroactic anhydride / 1) dichloromethane, -61 deg C, 2.5 h, 2) room temp., overnight

With dihydrogen peroxide; toluene-4-sulfonic acid; acetic acid; trifluoroacetic anhydride; In dichloromethane; toluene;