Technology Process of C63H56N2O4
There total 3 articles about C63H56N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
p-iodobenzoic acid pent-1-ene ester;
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine;
In
tetrahydrofuran;
at 20 ℃;
for 5h;
(R)-C6H3(C6H4CCH)2CN2H(CHCH3C6H5)2;
With
triethylamine;
In
tetrahydrofuran;
at 20 ℃;
for 37h;
DOI:10.1039/c2ob27054d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dicyclohexyl-carbodiimide; dmap / chloroform / 72 h / 0 - 20 °C
2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 5 h / 20 °C
2.2: 37 h / 20 °C
With
dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; chloroform;
DOI:10.1039/c2ob27054d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dicyclohexyl-carbodiimide; dmap / chloroform / 72 h / 0 - 20 °C
2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 5 h / 20 °C
2.2: 37 h / 20 °C
With
dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; chloroform;
DOI:10.1039/c2ob27054d