N-(2-benzyloxyphenyl)-N-(3-methyl-2-butenyl)-2-(N-tert-butoxycarbonylamino)acetamide

Base Information

Chemical Name:N-(2-benzyloxyphenyl)-N-(3-methyl-2-butenyl)-2-(N-tert-butoxycarbonylamino)acetamide
CAS No.:237747-77-2
Molecular Formula:C₂₅H₃₂N₂O₄
Molecular Weight:424.54
Hs Code.:

Synonyms:N-(2-benzyloxyphenyl)-N-(3-methyl-2-butenyl)-2-(N-tert-butoxycarbonylamino)acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-benzyloxyphenyl)-N-(3-methyl-2-butenyl)-2-(N-tert-butoxycarbonylamino)acetamide

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Technology Process of N-(2-benzyloxyphenyl)-N-(3-methyl-2-butenyl)-2-(N-tert-butoxycarbonylamino)acetamide

There total 1 articles about N-(2-benzyloxyphenyl)-N-(3-methyl-2-butenyl)-2-(N-tert-butoxycarbonylamino)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 870-63-3
prenyl bromide

: 183180-09-8
N-(2-benzyloxyphenyl)-2-(N-tert-butoxycarbonylamino)acetamide

: 237747-77-2
N-(2-benzyloxyphenyl)-N-(3-methyl-2-butenyl)-2-(N-tert-butoxycarbonylamino)acetamide

Guidance literature:: With sodium hydride; Yield given; Multistep reaction; 1.) THF, 55 deg C, 1.5 h, 2.) THF, RT, overnight;
DOI:10.1248/cpb.47.755

Reference yield: 90.0%

: 237747-77-2
N-(2-benzyloxyphenyl)-N-(3-methyl-2-butenyl)-2-(N-tert-butoxycarbonylamino)acetamide

: 237747-78-3
N-(2-hydroxyphenyl)-N-(3-methylbutyl)-2-(N-tert-butoxycarbonylamino)acetamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 3h; under 760 Torr;
DOI:10.1248/cpb.47.755

Reference yield:

: 237747-77-2
N-(2-benzyloxyphenyl)-N-(3-methyl-2-butenyl)-2-(N-tert-butoxycarbonylamino)acetamide

: 237747-80-7
N-methyl-N-phenyl-2-<2-phenoxy>acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / H₂ / 5 percent Pd/C / methanol / 3 h / 760 Torr

2: 76 percent / K₂CO₃ / dimethylformamide / 3.5 h / 70 °C

3: 99 percent / TFA / CH₂Cl₂ / 1 h / 0 °C

With hydrogen; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.47.755