4-[2-(9,9-dibutyl-7-ethynyl-9H-fluoren-2-yl)ethynyl]-N,N-dihexylbenzeneamine

Base Information

Chemical Name:4-[2-(9,9-dibutyl-7-ethynyl-9H-fluoren-2-yl)ethynyl]-N,N-dihexylbenzeneamine
CAS No.:882512-34-7
Molecular Formula:C₄₃H₅₅N
Molecular Weight:585.916
Hs Code.:

Synonyms:4-[2-(9,9-dibutyl-7-ethynyl-9H-fluoren-2-yl)ethynyl]-N,N-dihexylbenzeneamine

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Chemical Property of 4-[2-(9,9-dibutyl-7-ethynyl-9H-fluoren-2-yl)ethynyl]-N,N-dihexylbenzeneamine

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Technology Process of 4-[2-(9,9-dibutyl-7-ethynyl-9H-fluoren-2-yl)ethynyl]-N,N-dihexylbenzeneamine

There total 6 articles about 4-[2-(9,9-dibutyl-7-ethynyl-9H-fluoren-2-yl)ethynyl]-N,N-dihexylbenzeneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 944146-43-4
{{9,9-dibutyl-7-{2-[4-(dihexylamino)phenyl]ethynyl}-9H-fluoren-2-yl}}-2-methyl-3-butyn-2-ol

: 882512-34-7
4-[2-(9,9-dibutyl-7-ethynyl-9H-fluoren-2-yl)ethynyl]-N,N-dihexylbenzeneamine

Guidance literature:: With potassium hydroxide; isopropyl alcohol; In toluene; for 1h; Heating;
DOI:10.1039/b517270e

Reference yield:

: 9,9-bis(n-butyl)-2,7-diiodofluorene

: 882512-34-7
4-[2-(9,9-dibutyl-7-ethynyl-9H-fluoren-2-yl)ethynyl]-N,N-dihexylbenzeneamine

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / Et₃N; CuI / Pd(PPh₃)2Cl₂ / toluene / 16 h / 40 °C

2: 44 percent / NaOH; isopropanol / toluene / 0.5 h / Heating

3: 37 percent / Et₃N; CuI / Pd(PPh₃)2Cl₂ / toluene / 3.5 h / 40 °C

4: 87 percent / KOH; isopropanol / toluene / 1 h / Heating

With potassium hydroxide; sodium hydroxide; copper(l) iodide; triethylamine; isopropyl alcohol; bis-triphenylphosphine-palladium(II) chloride; In toluene; 3: Sonogashira reaction;
DOI:10.1039/b517270e

Reference yield:

: 944146-42-3
4-(9,9-dibutyl-7-ethynyl-9H-fluoren-2-yl)-2-methyl-3-butyn-2-ol

: 882512-34-7
4-[2-(9,9-dibutyl-7-ethynyl-9H-fluoren-2-yl)ethynyl]-N,N-dihexylbenzeneamine

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / Et₃N; CuI / Pd(PPh₃)2Cl₂ / toluene / 3.5 h / 40 °C

2: 87 percent / KOH; isopropanol / toluene / 1 h / Heating

With potassium hydroxide; copper(l) iodide; triethylamine; isopropyl alcohol; bis-triphenylphosphine-palladium(II) chloride; In toluene; 1: Sonogashira reaction;
DOI:10.1039/b517270e