[Pd(4,4'-di-tert-butyl-2,2'-dipyridyl)(2-(2-trifluoromethyl)anilino-4,6-di-tert-butylphenol(-2H))]

Base Information

• Chemical Name: [Pd(4,4'-di-tert-butyl-2,2'-dipyridyl)(2-(2-trifluoromethyl)anilino-4,6-di-tert-butylphenol(-2H))]
• CAS No.: 927669-22-5
• Molecular Formula: C₃₉H₄₈F₃N₃OPd
• Molecular Weight: 738.245

Synonyms:[Pd(4,4'-di-tert-butyl-2,2'-dipyridyl)(2-(2-trifluoromethyl)anilino-4,6-di-tert-butylphenol(-2H))]

Chemical Property of [Pd(4,4'-di-tert-butyl-2,2'-dipyridyl)(2-(2-trifluoromethyl)anilino-4,6-di-tert-butylphenol(-2H))]

Chemical Property:

Purity/Quality:

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Technology Process of [Pd(4,4'-di-tert-butyl-2,2'-dipyridyl)(2-(2-trifluoromethyl)anilino-4,6-di-tert-butylphenol(-2H))]

There total 1 articles about [Pd(4,4'-di-tert-butyl-2,2'-dipyridyl)(2-(2-trifluoromethyl)anilino-4,6-di-tert-butylphenol(-2H))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cobaltocene (1277-43-6,78206-33-4) + [Pd(4,4'-di-tert-butyl-2,2'-dipyridyl)(OC6H2(tert-butyl)2NC6H4CF3)](PF6) → bis(cyclopentadienyl)cobalt(III) hexafluorophosphate (12427-42-8) + [Pd(4,4'-di-tert-butyl-2,2'-dipyridyl)(2-(2-trifluoromethyl)anilino-4,6-di-tert-butylphenol(-2H))] (927669-22-5)

Guidance literature:

In dichloromethane; addn. Cp2Co to dry, deaerated soln. of Pd(C5H3NC(CH3)3)2(OC6H2(C(CH3)3)2NC6H4CF3)(PF6) in CH2Cl2 under Ar with stirring for 1 h at 20°C; removal of solvent by evapn. in vac., redissolving in CH3OH; filtration,slow evapn. of solvent, crystn., elem. anal.;

DOI:10.1039/b614745c

upstream raw materials:

cobaltocene

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