2-(9,10-dihydro-9,10-diphenyl-9,10-epidioxyanthracenyl) tert-butyl nitroxide

Base Information

Chemical Name:2-(9,10-dihydro-9,10-diphenyl-9,10-epidioxyanthracenyl) tert-butyl nitroxide
CAS No.:103438-70-6
Molecular Formula:C₃₀H₂₆NO₃
Molecular Weight:448.541
Hs Code.:

Synonyms:2-(9,10-dihydro-9,10-diphenyl-9,10-epidioxyanthracenyl) tert-butyl nitroxide

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Chemical Property of 2-(9,10-dihydro-9,10-diphenyl-9,10-epidioxyanthracenyl) tert-butyl nitroxide

Chemical Property:

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Technology Process of 2-(9,10-dihydro-9,10-diphenyl-9,10-epidioxyanthracenyl) tert-butyl nitroxide

There total 3 articles about 2-(9,10-dihydro-9,10-diphenyl-9,10-epidioxyanthracenyl) tert-butyl nitroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 103438-61-5
2-(9,10-diphenylanthracenyl)-tert-butyl nitroxide

: 103438-70-6
2-(9,10-dihydro-9,10-diphenyl-9,10-epidioxyanthracenyl) tert-butyl nitroxide

Guidance literature:: With air; methylene blue; In dichloromethane; at 10 - 15 ℃; for 2.5h; Irradiation;
DOI:10.1021/jo00368a010

Reference yield:

: 43217-28-3
2-chloro-9,10-diphenylanthracene

: 103438-70-6
2-(9,10-dihydro-9,10-diphenyl-9,10-epidioxyanthracenyl) tert-butyl nitroxide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg / 1.) THF, -78 to 25 deg C, 2 h, 2.) THF, 25 deg C, 12 h

2: 96 percent / K₃Fe(CN)6, aq. NaOH / CH₂Cl₂ / 0.25 h

3: 52 percent / methylene blue, air / CH₂Cl₂ / 2.5 h / 10 - 15 °C / Irradiation

With sodium hydroxide; air; methylene blue; magnesium; potassium hexacyanoferrate(III); In dichloromethane;
DOI:10.1021/jo00368a010

Reference yield:

: 103438-67-1
N-<2-(9,10-diphenylanthracenyl)>-N-tert-butylhydroxyloamine

: 103438-70-6
2-(9,10-dihydro-9,10-diphenyl-9,10-epidioxyanthracenyl) tert-butyl nitroxide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / K₃Fe(CN)6, aq. NaOH / CH₂Cl₂ / 0.25 h

2: 52 percent / methylene blue, air / CH₂Cl₂ / 2.5 h / 10 - 15 °C / Irradiation

With sodium hydroxide; air; methylene blue; potassium hexacyanoferrate(III); In dichloromethane;
DOI:10.1021/jo00368a010