Technology Process of C26H32O4
There total 9 articles about C26H32O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanol; sodium tetrahydroborate; cerium(III) chloride heptahydrate;
at 20 ℃;
for 0.333333h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: n-butyllithium / tetrahydrofuran; hexanes / 0.58 h / -78 °C
1.2: -78 °C
2.1: dihydrogen peroxide / Shi's ketone / ethanol; dichloromethane; water; acetonitrile / 9 h / 0 °C / aq buffer (2 M K2CO3 and 4 mM EDTA)
3.1: boron trifluoride diethyl etherate / dichloromethane / 0.12 h / -78 °C
4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 18.5 h / 20 °C
5.1: potassium hydroxide / ethanol / 2 h / 20 °C
6.1: methanol; sodium tetrahydroborate; cerium(III) chloride heptahydrate / 0.33 h / 20 °C
With
methanol; sodium tetrahydroborate; n-butyllithium; tetrapropylammonium perruthennate; cerium(III) chloride heptahydrate; boron trifluoride diethyl etherate; dihydrogen peroxide; 4-methylmorpholine N-oxide; potassium hydroxide;
Shi's ketone;
In
tetrahydrofuran; hexanes; ethanol; dichloromethane; water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: n-butyllithium / tetrahydrofuran; hexanes / 0.58 h / -78 °C
1.2: -78 °C
2.1: dihydrogen peroxide / Shi's ketone / ethanol; dichloromethane; water; acetonitrile / 9 h / 0 °C / aq buffer (2 M K2CO3 and 4 mM EDTA)
3.1: boron trifluoride diethyl etherate / dichloromethane / 0.12 h / -78 °C
4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 18.5 h / 20 °C
5.1: potassium hydroxide / ethanol / 2 h / 20 °C
6.1: methanol; sodium tetrahydroborate; cerium(III) chloride heptahydrate / 0.33 h / 20 °C
With
methanol; sodium tetrahydroborate; n-butyllithium; tetrapropylammonium perruthennate; cerium(III) chloride heptahydrate; boron trifluoride diethyl etherate; dihydrogen peroxide; 4-methylmorpholine N-oxide; potassium hydroxide;
Shi's ketone;
In
tetrahydrofuran; hexanes; ethanol; dichloromethane; water; acetonitrile;