p-methoxyphenyl 2,3-O-isopropylidene-α-L-rhamnopyranosyl-(1->2)-3,4-O-isopropylidene-β-D-fucopyranoside

Base Information

Chemical Name:p-methoxyphenyl 2,3-O-isopropylidene-α-L-rhamnopyranosyl-(1->2)-3,4-O-isopropylidene-β-D-fucopyranoside
CAS No.:1252047-39-4
Molecular Formula:C₂₅H₃₆O₁₀
Molecular Weight:496.555
Hs Code.:

Synonyms:p-methoxyphenyl 2,3-O-isopropylidene-α-L-rhamnopyranosyl-(1->2)-3,4-O-isopropylidene-β-D-fucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-methoxyphenyl 2,3-O-isopropylidene-α-L-rhamnopyranosyl-(1->2)-3,4-O-isopropylidene-β-D-fucopyranoside

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Technology Process of p-methoxyphenyl 2,3-O-isopropylidene-α-L-rhamnopyranosyl-(1->2)-3,4-O-isopropylidene-β-D-fucopyranoside

There total 1 articles about p-methoxyphenyl 2,3-O-isopropylidene-α-L-rhamnopyranosyl-(1->2)-3,4-O-isopropylidene-β-D-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1252047-38-3
p-methoxyphenyl 4-O-acetyl-2,3-O-isopropylidene-α-L-rhamnopyranosyl-(1->2)-3,4-O-isopropylidene-β-D-fucopyranoside

: 1252047-39-4
p-methoxyphenyl 2,3-O-isopropylidene-α-L-rhamnopyranosyl-(1->2)-3,4-O-isopropylidene-β-D-fucopyranoside

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 2h;
DOI:10.1016/j.tetasy.2010.06.032

Reference yield: 89.0%

: 1252047-39-4
p-methoxyphenyl 2,3-O-isopropylidene-α-L-rhamnopyranosyl-(1->2)-3,4-O-isopropylidene-β-D-fucopyranoside

: 824-94-2
p-methoxybenzyl chloride

: p-methoxyphenyl 2,3-O-isopropylidene-4-O-(4-methoxybenzyl)-α-L-rhamnopyranosyl-(1→2)-3,4-O-isopropylidene-β-D-fucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 1h;
DOI:10.1080/07328303.2015.1069829

Reference yield: 74.0%

: 1252047-39-4
p-methoxyphenyl 2,3-O-isopropylidene-α-L-rhamnopyranosyl-(1->2)-3,4-O-isopropylidene-β-D-fucopyranoside

: 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl-(1->3)-2,4-di-O-acetyl-D-xylopyranosyl trichloroacetimidate

: 1252047-45-2
p-methoxyphenyl 2,3,4-tri-O-acetyl-α-L-rhamnopyranosyl-(1->3)-2,4-di-O-acetyl-β-D-xylopyranosyl-(1->4)-2,3-O-isopropylidene-α-L-rhamnopyranosyl-(1->2)-3,4-O-isopropylidene-β-D-fucopyranoside

Guidance literature:: With silica-gel-supported sulfuric acid; In dichloromethane; at 20 ℃; for 2h; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tetasy.2010.06.032