C₅₇H₈₀O₈Si₂

Base Information

Chemical Name:C₅₇H₈₀O₈Si₂
CAS No.:1427032-03-8
Molecular Formula:C₅₇H₈₀O₈Si₂
Molecular Weight:949.428
Hs Code.:

C<sub>57</sub>H<sub>80</sub>O<sub>8</sub>Si<sub>2</sub>

Synonyms:C₅₇H₈₀O₈Si₂

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Chemical Property of C₅₇H₈₀O₈Si₂

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Technology Process of C₅₇H₈₀O₈Si₂

There total 13 articles about C₅₇H₈₀O₈Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₃₁Cl₃O₇

: 1427031-92-2
C₃₂H₅₂O₃Si₂

: 1427032-03-8
C₅₇H₈₀O₈Si₂

Guidance literature:: With dmap; In toluene; at 20 ℃; for 1.5h;
DOI:10.1021/ol400408w

Reference yield:

: C₃₁H₄₂O₅Si

: 1427032-03-8
C₅₇H₈₀O₈Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: sodium periodate / tetrahydrofuran; water / 1 h / 20 °C

2: toluene / 1.33 h / -78 - 20 °C / Molecular sieve

3: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 0 - 20 °C / pH 7

5: diethylazodicarboxylate; triphenylphosphine / toluene; tetrahydrofuran / 2 h / 0 - 20 °C

6: diisobutylaluminium hydride / dichloromethane; hexane / 1 h / -78 °C

7: dmap / toluene / 1.5 h / 20 °C

With 2,6-dimethylpyridine; dmap; sodium periodate; diisobutylaluminium hydride; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; diethylazodicarboxylate; In tetrahydrofuran; hexane; dichloromethane; water; toluene; 5: |Mitsunobu Displacement;
DOI:10.1021/ol400408w

Reference yield:

: C₂₃H₃₆O₅Si

: 1427032-03-8
C₅₇H₈₀O₈Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: pyridinium p-toluenesulfonate / methanol / 22 h / 20 °C

2: lanthanum(lll) triflate / toluene / 1 h / 20 °C

3: lithium hydroxide monohydrate / tetrahydrofuran; water; methanol / 0 - 20 °C

4: triethylamine / tetrahydrofuran / 0.83 h / 0 - 20 °C

5: dmap / toluene / 1.5 h / 20 °C

With dmap; lithium hydroxide monohydrate; pyridinium p-toluenesulfonate; triethylamine; lanthanum(lll) triflate; In tetrahydrofuran; methanol; water; toluene; 4: |Yamaguchi Lactonization;
DOI:10.1021/ol400408w