C₂₉H₅₄O₅Si₂

Base Information

Chemical Name:C₂₉H₅₄O₅Si₂
CAS No.:1395502-77-8
Molecular Formula:C₂₉H₅₄O₅Si₂
Molecular Weight:538.916
Hs Code.:

C<sub>29</sub>H<sub>54</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₂₉H₅₄O₅Si₂

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Chemical Property of C₂₉H₅₄O₅Si₂

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Technology Process of C₂₉H₅₄O₅Si₂

There total 8 articles about C₂₉H₅₄O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1395502-35-8
C₃₁H₅₆O₆Si₂

: 1395502-77-8
C₂₉H₅₄O₅Si₂

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol302072b

Reference yield:

: 847049-72-3
1-methoxy-4-{[(2S)-pent-4-en-2-yloxy]methyl}benzene

: 1395502-77-8
C₂₉H₅₄O₅Si₂

Guidance literature:: Multi-step reaction with 8 steps

1: sodium periodate; osmium(VIII) oxide; 2,6-dimethylpyridine / 1,4-dioxane; water / 20 °C / Inert atmosphere

2: toluene / 5 h / 80 °C / Inert atmosphere

3: AD-mix-α; methanesulfonamide / 1,4-dioxane; water / 48 h / 0 °C / Inert atmosphere

4: pyridine; silver nitrate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

5: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C / Inert atmosphere

6: N-ethyl-N,N-diisopropylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1.5 h / 20 °C / Inert atmosphere

7: toluene / 90 °C / Inert atmosphere

8: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; methanesulfonamide; AD-mix-α; sulfur trioxide pyridine complex; diisobutylaluminium hydride; silver nitrate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; 2: |Horner-Wadsworth-Emmons Olefination / 7: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/ol302072b

Reference yield:

: 1395502-34-7
C₁₅H₂₀O₄

: 1395502-77-8
C₂₉H₅₄O₅Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: AD-mix-α; methanesulfonamide / 1,4-dioxane; water / 48 h / 0 °C / Inert atmosphere

2: pyridine; silver nitrate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

3: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C / Inert atmosphere

4: N-ethyl-N,N-diisopropylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 1.5 h / 20 °C / Inert atmosphere

5: toluene / 90 °C / Inert atmosphere

6: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C / Inert atmosphere

With pyridine; methanesulfonamide; AD-mix-α; sulfur trioxide pyridine complex; diisobutylaluminium hydride; silver nitrate; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; 5: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/ol302072b