2-(3-(trifluoromethyl)phenyl)benzo[d]oxazole

Base Information

• Chemical Name: 2-(3-(trifluoromethyl)phenyl)benzo[d]oxazole
• CAS No.: 15952-19-9
• Molecular Formula: C₁₄H₈F₃NO
• Molecular Weight: 263.219

Synonyms:2-(3-(trifluoromethyl)phenyl)benzo[d]oxazole

Chemical Property of 2-(3-(trifluoromethyl)phenyl)benzo[d]oxazole

Chemical Property:

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Technology Process of 2-(3-(trifluoromethyl)phenyl)benzo[d]oxazole

There total 12 articles about 2-(3-(trifluoromethyl)phenyl)benzo[d]oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C14H9BrF3NO → 2-(3-(trifluoromethyl)phenyl)benzo[d]oxazole (15952-19-9)

Guidance literature:

With copper(l) iodide; 4-phenyl-1-(3-O-benzyl-6-deoxy-1,2-O-isopropylidene-α-D-glucofuranos-6-yl)-1H-1,2,3-triazole; potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 10h; Inert atmosphere; Sealed tube;

DOI:10.1021/acscombsci.9b00004

Reference yield: 91.0%

benzoxazole (273-53-0,29791-96-6) + 3-(Trifluoromethyl)benzoyl chloride (2251-65-2) → 2-(3-(trifluoromethyl)phenyl)benzo[d]oxazole (15952-19-9)

Guidance literature:

With potassium carbonate; In water; chlorobenzene; at 140 ℃; for 24h; Sealed tube;

DOI:10.1021/jo402106q

Reference yield: 87.0%

benzoxazole (273-53-0,29791-96-6) + 3-(trifluoromethyl)benzenesulfonylhydrazide (890522-54-0) → 2-(3-(trifluoromethyl)phenyl)benzo[d]oxazole (15952-19-9)

Guidance literature:

With dichloro bis(acetonitrile) palladium(II); 1,10-Phenanthroline; tetrabutylammomium bromide; copper diacetate; sodium carbonate; In 1,4-dioxane; dimethyl sulfoxide; at 20 - 100 ℃; for 4.58333h; Inert atmosphere;

DOI:10.1039/c2ob26270c

upstream raw materials:

N-(2-Hydroxy-phenyl)-3-trifluoromethyl-benzamide

benzoxazole

3-(trifluoromethyl)phenyl methanesulfonate

3-(trifluoromethyl)phenyl 4-methylbenzenesulfonate

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