C-2-(benzyloxy)ethyl-C'-aminomethyl-o-carborane

Base Information

Chemical Name:C-2-(benzyloxy)ethyl-C'-aminomethyl-o-carborane
CAS No.:1096253-48-3
Molecular Formula:C₁₂H₂₅B₁₀NO
Molecular Weight:307.447
Hs Code.:

Synonyms:C-2-(benzyloxy)ethyl-C'-aminomethyl-o-carborane

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Chemical Property of C-2-(benzyloxy)ethyl-C'-aminomethyl-o-carborane

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Technology Process of C-2-(benzyloxy)ethyl-C'-aminomethyl-o-carborane

There total 1 articles about C-2-(benzyloxy)ethyl-C'-aminomethyl-o-carborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1096253-46-1
C-2-(benzyloxy)ethyl-C'-tert-butoxyamidomethyl-o-carborane

: 76-05-1
trifluoroacetic acid

: 1096253-48-3
C-2-(benzyloxy)ethyl-C'-aminomethyl-o-carborane

Guidance literature:: In dichloromethane; trifluoroacetic acid; addn. of CF3COOH to carborane deriv. in anhyd. CH2Cl2, stirring for 2 h at room temp.; addn. of brine, extn. (CH2Cl2), washing CH2Cl2 phase with brine, drying,evapn., elem. anal.;
DOI:10.1039/b808804g

Reference yield: 73.0%

: 3-(cholesten-5-en-3β-yloxy)propionic acid

: 1096253-48-3
C-2-(benzyloxy)ethyl-C'-aminomethyl-o-carborane

: C-(2-benzyloxyethyl)-C'-[cholesten-5-en-3β-yloxy-(3-propionacetoamidomethyl)]-o-carborane

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1039/c3ob42414f

Reference yield: 64.0%

: 1096253-48-3
C-2-(benzyloxy)ethyl-C'-aminomethyl-o-carborane

: 57-10-3
1-hexadecylcarboxylic acid

: 1096253-49-4
C-2-(benzyloxy)ethyl-C'-palmitamidomethyl-o-carborane

Guidance literature:: With (CH₃O)2C₂N₃Cl; N-methylmorpholine; In dichloromethane; addn. of amine deriv. to soln. of palmitic acid and triazine deriv. in CH2Cl2 at -5-0°C, stirring at 0°C for 4 h, addn. of CH2Cl2 soln. of carborane deriv. and amine deriv., keeping at 0°C for 2 h, keeping at room temp. overnight; evapn., addn. of CH2Cl2, washing with water, aq. citric acid, satd. aq. NaHCO3 and water, drying, evapn., chromy. (silica gel, CH2Cl2), elem. anal.;
DOI:10.1039/b808804g