Methyl 4-<2-exo,6-exo-6-(3,4-dimethoxyphenyl)-7-oxa-1-azabicyclo<2.2.1>heptan-2-yl>butanoate

Base Information

Chemical Name:Methyl 4-<2-exo,6-exo-6-(3,4-dimethoxyphenyl)-7-oxa-1-azabicyclo<2.2.1>heptan-2-yl>butanoate
CAS No.:102652-47-1
Molecular Formula:C₁₈H₂₅NO₅
Molecular Weight:335.4
Hs Code.:

Synonyms:Methyl 4-<2-exo,6-exo-6-(3,4-dimethoxyphenyl)-7-oxa-1-azabicyclo<2.2.1>heptan-2-yl>butanoate

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Chemical Property of Methyl 4-<2-exo,6-exo-6-(3,4-dimethoxyphenyl)-7-oxa-1-azabicyclo<2.2.1>heptan-2-yl>butanoate

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Technology Process of Methyl 4-<2-exo,6-exo-6-(3,4-dimethoxyphenyl)-7-oxa-1-azabicyclo<2.2.1>heptan-2-yl>butanoate

There total 1 articles about Methyl 4-<2-exo,6-exo-6-(3,4-dimethoxyphenyl)-7-oxa-1-azabicyclo<2.2.1>heptan-2-yl>butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102652-46-0
C₁₈H₂₅NO₅

: 102652-47-1
Methyl 4-<2-exo,6-exo-6-(3,4-dimethoxyphenyl)-7-oxa-1-azabicyclo<2.2.1>heptan-2-yl>butanoate

: 102734-21-4
Methyl 4-<2-exo,6-endo-6-(3,4-dimethoxyphenyl)-7-oxa-1-azabicyclo<2.2.1>heptan-2-yl>butanoate

: 102734-20-3
Methyl 4-<2-endo,6-exo-6-(3,4-dimethoxyphenyl)-7-oxa-1-azabicyclo<2.2.1>heptan-2-yl>butanoate

Guidance literature:: In xylene; for 1h; Yield given. Yields of byproduct given; Heating;

Reference yield: 95.0%

: 102652-47-1
Methyl 4-<2-exo,6-exo-6-(3,4-dimethoxyphenyl)-7-oxa-1-azabicyclo<2.2.1>heptan-2-yl>butanoate

: 102652-51-7
Methyl 4-butanoate

Guidance literature:: With acetic acid; zinc; at 65 ℃; for 4h;

Reference yield:

: 102652-47-1
Methyl 4-<2-exo,6-exo-6-(3,4-dimethoxyphenyl)-7-oxa-1-azabicyclo<2.2.1>heptan-2-yl>butanoate

: 89771-49-3
(±)-lasubine II

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / Zn(powder)/CH₃COOH(80percent) / 4 h / 65 °C

2: 1) (trimethylsilyl)imidazole, 2) 2-pyridinol, 1 M (C₄H₉)4NF in THF / 1) 4 h, CH₂Cl₂, 2) 2 h, 160 deg C

3: 74 percent / triphenylphosphane/benzoic acid/diethyl azodicarboxylate / CH₂Cl₂ / 48 h / Ambient temperature

4: 76 percent / LAH / tetrahydrofuran / 4 h / Heating

With 2-hydroxypyridin; lithium aluminium tetrahydride; tetrabutyl ammonium fluoride; acetic acid; 1-(Trimethylsilyl)imidazole; triphenylphosphine; benzoic acid; zinc; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane;