(E)-N-(1-cyclohexyl-2-methyl-but-2-enyl)-4-methyl-benzenesulfonamide

Base Information

• Chemical Name: (E)-N-(1-cyclohexyl-2-methyl-but-2-enyl)-4-methyl-benzenesulfonamide
• CAS No.: 945933-25-5
• Molecular Formula: C₁₈H₂₇NO₂S
• Molecular Weight: 321.484
• Mol file: 945933-25-5.mol

Synonyms:(E)-N-(1-cyclohexyl-2-methyl-but-2-enyl)-4-methyl-benzenesulfonamide

Chemical Property of (E)-N-(1-cyclohexyl-2-methyl-but-2-enyl)-4-methyl-benzenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-N-(1-cyclohexyl-2-methyl-but-2-enyl)-4-methyl-benzenesulfonamide

There total 1 articles about (E)-N-(1-cyclohexyl-2-methyl-but-2-enyl)-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethylacetylene (503-17-3) + (E)-N-cyclohexylmethylene-4-toluenesulfonamide (260975-29-9) → (E)-N-(1-cyclohexyl-2-methyl-but-2-enyl)-4-methyl-benzenesulfonamide (945933-25-5) + (Z)-N-(1-cyclohexyl-2-methyl-but-2-enyl)-4-methyl-benzenesulfonamide

Guidance literature:

With hydrogen; sodium sulfate; Ir(cod)2BARF; triphenylacetic acid; In toluene; at 60 ℃; for 24h; under 760.051 Torr; Title compound not separated from byproducts.;

DOI:10.1021/ja073018j

Reference yield:

(E)-N-(1-cyclohexyl-2-methyl-but-2-enyl)-4-methyl-benzenesulfonamide (945933-25-5) → C11H21N

Guidance literature:

With sodium naphthalenide; In 1,2-dimethoxyethane; at 20 ℃; for 1h;

DOI:10.1021/ja073018j

Reference yield:

(E)-N-(1-cyclohexyl-2-methyl-but-2-enyl)-4-methyl-benzenesulfonamide (945933-25-5) → (E)-benzyl 1-cyclohexyl-2-methylbut-2-enylcarbamate

Guidance literature:

Multi-step reaction with 2 steps

1: sodium naphthalenide / 1,2-dimethoxy-ethane / 1 h / 20 °C

2: aq. Na₂CO₃ / ethyl acetate / 2 h / 20 °C

With sodium naphthalenide; sodium carbonate; In 1,2-dimethoxyethane; ethyl acetate;

DOI:10.1021/ja073018j

upstream raw materials:

dimethylacetylene

(E)-N-cyclohexylmethylene-4-toluenesulfonamide